BMRB: 10002

F-spondin TSR 4

Authors

Paakkonen, K., Tossavainen, H., Permi, P., Rakkolainen, H., Rauvala, H., Raulo, E., Kilpelainen, I., Guntert, P.

Assembly

F-spondin TSR4

Entity

1. F-spondin TSR4 (polymer, Thiol state: all disulfide bound), 56 monomers, 6234.144 Da Detail

GSIPCLLSPW SEWSDCSVTC GKGMRTRQRM LKSLAELGDC NEDLEQAEKC MLPECP

Formula weight

6234.144 Da

Source organism

Rattus norvegicus

Exptl. method

NMR

Refine. method

TORSION ANGLE DYNAMICS

Data set

assigned_chemical_shifts

Chem. Shift Complete

Sequence coverage: 98.2 %, Completeness: 95.9 %, Completeness (bb): 93.9 % Detail

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Polymer type: polypeptide(L)

	Total	1H	13C	15N
All	95.9 % (601 of 627)	96.7 % (320 of 331)	94.6 % (226 of 239)	96.5 % (55 of 57)
Backbone	93.9 % (308 of 328)	93.8 % (105 of 112)	93.3 % (153 of 164)	96.2 % (50 of 52)
Sidechain	98.0 % (344 of 351)	98.2 % (215 of 219)	97.6 % (124 of 127)	100.0 % (5 of 5)
Aromatic	100.0 % (24 of 24)	100.0 % (12 of 12)	100.0 % (10 of 10)	100.0 % (2 of 2)
Methyl	97.7 % (43 of 44)	100.0 % (22 of 22)	95.5 % (21 of 22)

1. F-spondin TSR 4

GSIPCLLSPW SEWSDCSVTC GKGMRTRQRM LKSLAELGDC NEDLEQAEKC MLPECP

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Sample

Temperature 283 (±0.1) K, pH 6.8 (±0.1)

#	Name	Isotope labeling	Type	Concentration
1	F-spondin TSR 4			0.0 ~ 0.0 mM

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LACS Plot; CA

Referencing offset: -0.49 ppm, Outliers: 1 Detail

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Chemical shift reference

Atom type	Mol. common name	Atom group	Value	Ref. method	Ref. type	Shift ratio
1H	water	protons	4.9 ppm	internal	indirect	0.0

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LACS Plot; CB

Referencing offset: -0.49 ppm, Outliers: 1 Detail

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Chemical shift reference

Atom type	Mol. common name	Atom group	Value	Ref. method	Ref. type	Shift ratio
1H	water	protons	4.9 ppm	internal	indirect	0.0

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LACS Plot; HA

Referencing offset: 0.08 ppm, Outliers: 1 Detail

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Chemical shift reference

Atom type	Mol. common name	Atom group	Value	Ref. method	Ref. type	Shift ratio
1H	water	protons	4.9 ppm	internal	indirect	0.0

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LACS Plot; CO

Referencing offset: 0.1 ppm, Outliers: 1 Detail

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Chemical shift reference

Atom type	Mol. common name	Atom group	Value	Ref. method	Ref. type	Shift ratio
1H	water	protons	4.9 ppm	internal	indirect	0.0

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Protein Blocks Logo

Calculated from 20 models in PDB: 1VEX, Strand ID: A Detail

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Release date

2006-06-27

Citation

Solution structures of the first and fourth TSR domains of F-spondin
Paakkonen, K., Tossavainen, H., Permi, P., Rakkolainen, H., Rauvala, H., Raulo, E., Kilpelainen, I., Guntert, P.
Proteins (2006), 64, 665-672, PubMed 16736493 , DOI 10.1002/prot.21030 , Abstract

Entries sharing articles BMRB: 1, Swiss-Prot: 1 entries Detail

Related entities 1. F-spondin TSR4, : 1 : 334 entities Detail

Interaction partners 1. F-spondin TSR4, : 7 interactors Detail