Solution Structure of the C-terminal Pleckstrin Homology Domain of Sbf1 from Mouse
GSSGSSGRSY EGILYKKGAF MKPWKARWFV LDKTKHQLRY YDHRMDTECK GVIDLAEVEA VAPGTPTIGA PKTVDEKAFF DVKTTRRVYN FCAQDVPSAQ QWVDRIQSCL SSGPSSG
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 96.4 % (1301 of 1350) | 95.4 % (671 of 703) | 97.0 % (511 of 527) | 99.2 % (119 of 120) |
Backbone | 97.5 % (673 of 690) | 95.8 % (228 of 238) | 98.2 % (335 of 341) | 99.1 % (110 of 111) |
Sidechain | 95.6 % (733 of 767) | 95.3 % (443 of 465) | 95.9 % (281 of 293) | 100.0 % (9 of 9) |
Aromatic | 92.5 % (124 of 134) | 92.5 % (62 of 67) | 92.2 % (59 of 64) | 100.0 % (3 of 3) |
Methyl | 100.0 % (104 of 104) | 100.0 % (52 of 52) | 100.0 % (52 of 52) |
1. The Pleckstrin Homology Domain
GSSGSSGRSY EGILYKKGAF MKPWKARWFV LDKTKHQLRY YDHRMDTECK GVIDLAEVEA VAPGTPTIGA PKTVDEKAFF DVKTTRRVYN FCAQDVPSAQ QWVDRIQSCL SSGPSSGPressure 1 (±0.001) atm, Temperature 298 (±0.1) K, pH 6.0 (±0.05)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Pleckstrin Homology domain | [U-13C; U-15N] | 0.28 mM | |
2 | PiNa | 20 mM | ||
3 | NaCl | salt | 100 mM | |
4 | d-DTT | salt | 1 mM | |
5 | NaN3 | 0.02 % | ||
6 | H2O | solvent | 90 % | |
7 | D2O | solvent | 10 % |