BMRBj - BMREntryMaster

	Total	¹H	¹³C	¹⁵N
All	65.6 % (857 of 1306)	58.4 % (398 of 681)	71.7 % (365 of 509)	81.0 % (94 of 116)
Backbone	92.1 % (595 of 646)	89.3 % (200 of 224)	95.3 % (302 of 317)	88.6 % (93 of 105)
Sidechain	47.0 % (357 of 759)	43.3 % (198 of 457)	54.3 % (158 of 291)	9.1 % (1 of 11)
Aromatic	26.5 % (36 of 136)	33.8 % (23 of 68)	17.9 % (12 of 67)	100.0 % (1 of 1)
Methyl	65.7 % (71 of 108)	63.0 % (34 of 54)	68.5 % (37 of 54)

1. gp16

MYEEFRDVIT FQSYVEQSNG EGGKTYKWVD EFTAAAHVQP ISQEEYYKAQ QLQTPIGYNI YTPYDDRIDK KMRVIYRGKI VTFIGDPVDL SGLQEITRIK GKEDGAYVG

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.5

#	Name	Isotope labeling	Concentration
1	gp16	natural abundance	0.35 mM
2	HEPES	natural abundance	5 mM
3	sodium chloride	natural abundance	300 mM
4	H2O	natural abundance	90 %
5	D2O	natural abundance	10 %

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.5

#	Name	Isotope labeling	Concentration
6	gp16	[U-100% 15N]	0.35 mM
7	HEPES	natural abundance	5 mM
8	sodium chloride	natural abundance	300 mM
9	H2O	natural abundance	90 %
10	D2O	natural abundance	10 %

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.5

#	Name	Isotope labeling	Concentration
11	gp16	[U-100% 13C; U-100% 15N]	0.35 mM
12	HEPES	natural abundance	5 mM
13	sodium chloride	natural abundance	300 mM
14	H2O	natural abundance	90 %
15	D2O	natural abundance	10 %

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.5

#	Name	Isotope labeling	Concentration
16	gp16	[U-100% 13C; U-100% 15N; U-80% 2H]	0.35 mM
17	HEPES	natural abundance	5 mM
18	sodium chloride	natural abundance	300 mM
19	H2O	natural abundance	90 %
20	D2O	natural abundance	10 %

LACS Plot; CA

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	TSP	methyl protons	internal	indirect	0.2514495
¹H	TSP	methyl protons	internal	direct	1.0
¹⁵N	TSP	methyl protons	internal	indirect	0.1013291

Referencing offset: 0.3 ppm, Outliers: 1 Detail

LACS Plot; CB

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	TSP	methyl protons	internal	indirect	0.2514495
¹H	TSP	methyl protons	internal	direct	1.0
¹⁵N	TSP	methyl protons	internal	indirect	0.1013291

Referencing offset: 0.3 ppm, Outliers: 1 Detail

LACS Plot; HA

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	TSP	methyl protons	internal	indirect	0.2514495
¹H	TSP	methyl protons	internal	direct	1.0
¹⁵N	TSP	methyl protons	internal	indirect	0.1013291

Referencing offset: -0.04 ppm, Outliers: 5 Detail

LACS Plot; CO

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	TSP	methyl protons	internal	indirect	0.2514495
¹H	TSP	methyl protons	internal	direct	1.0
¹⁵N	TSP	methyl protons	internal	indirect	0.1013291

Referencing offset: 0.74 ppm, Outliers: 1 Detail

Protein Blocks Logo

Calculated from 20 models in PDB: 2KCA, Strand ID: A Detail

Release date

2009-05-19

Citation

Structure of bacteriophage SPP1 head-to-tail connection reveals mechanism for viral DNA gating
Lhuillier, S., Gallopin, M., Gilquin, B., Brasiles, S., Lancelot, N., Letellier, G., Gilles, M., Dethan, G., Orlova, E.V., Couprie, J., Tavares, P., Zinn-Justin, S.
Proc. Natl. Acad. Sci. U. S. A. (2009), 106, 8507-8512, PubMed 19433794 , DOI 10.1073/pnas.0812407106 , Abstract