BMRB: 16605

MAUROCALCINE IN D CONFIGURATION FROM SCORPIO MAURUS PALMATUS

Authors

Dridi, K., Bernard, C., Darbon, H.

Assembly

MAUROCALCINE

Entity

1. MAUROCALCINE (polymer, Thiol state: all disulfide bound), 33 monomers, 3864.595 Da Detail

GDCLPHLKLC KENKDCCSKK CKRRGTNIEK RCR

Formula weight

3864.595 Da

Entity Connection

disulfide 3 Detail

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ID	Type	Value order	Atom ID 1	Atom ID 2
1	disulfide	sing	1:CYS3:SG	1:CYS17:SG
2	disulfide	sing	1:CYS10:SG	1:CYS21:SG
3	disulfide	sing	1:CYS16:SG	1:CYS32:SG

Exptl. method

solution NMR

Data set

assigned_chemical_shifts

Chem. Shift Complete

Sequence coverage: 100.0 %, Completeness: 98.2 %, Completeness (bb): 95.5 % Detail

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Polymer type: polypeptide(D)

	Total	1H
All	98.2 % (213 of 217)	98.2 % (213 of 217)
Backbone	95.5 % (64 of 67)	95.5 % (64 of 67)
Sidechain	99.3 % (149 of 150)	99.3 % (149 of 150)
Aromatic	100.0 % (2 of 2)	100.0 % (2 of 2)
Methyl	100.0 % (9 of 9)	100.0 % (9 of 9)

1. D-MAUROCALCINE

GDCLPHLKLC KENKDCCSKK CKRRGTNIEK RCR

Show sample condition

Sample #1

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 300 K, pH 7

#	Name	Isotope labeling	Type	Concentration
1	D-MAUROCALCINE	natural abundance		4 mg
2	H2O	natural abundance		90 %
3	D2O	natural abundance		10 %

Sample #2

Solvent system 100% D2O, Pressure 1 atm, Temperature 300 K, pH 7

#	Name	Isotope labeling	Type	Concentration
4	D-MAUROCALCINE	natural abundance		4 mg
5	D2O	natural abundance		100 %

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Release date

2010-06-23

Citation

D-Maurocalcine, a pharmacologically inert efficient cell-penetrating peptide analogue
Poillot, C., Dridi, K., Bichraoui, H., Pecher, J., Alphonse, S., Douzi, B., Ronjat, M., Darbon, H., De Waard, M.
J. Biol. Chem. (2010), 285, 34168-34180, PubMed 20610396 , DOI 10.1074/jbc.M110.104919 , Abstract

Related entities 1. MAUROCALCINE, : 2 : 3 : 6 entities Detail

Experiments performed 4 experiments Detail