Solution structure of the N-terminal domain (residues 1-111) of Brugia malayi asparaginyl-tRNA synthetase
GSMTVYICPE TGDDGNDGSE LKPLRTLYQA MIITKSSKGD FLIRTKKDGK QVWEAASKTA LKKSWKRYEQ EMLKNEKVAA KMLEKDATEV GVKAALEEAK KVQIELDTSL SYI
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 96.9 % (1292 of 1333) | 97.6 % (682 of 699) | 95.3 % (491 of 515) | 100.0 % (119 of 119) |
Backbone | 99.1 % (668 of 674) | 99.1 % (229 of 231) | 98.8 % (328 of 332) | 100.0 % (111 of 111) |
Sidechain | 93.7 % (717 of 765) | 95.1 % (445 of 468) | 91.3 % (264 of 289) | 100.0 % (8 of 8) |
Aromatic | 65.2 % (43 of 66) | 78.8 % (26 of 33) | 48.4 % (15 of 31) | 100.0 % (2 of 2) |
Methyl | 100.0 % (124 of 124) | 100.0 % (62 of 62) | 100.0 % (62 of 62) |
1. AsnRS
GSMTVYICPE TGDDGNDGSE LKPLRTLYQA MIITKSSKGD FLIRTKKDGK QVWEAASKTA LKKSWKRYEQ EMLKNEKVAA KMLEKDATEV GVKAALEEAK KVQIELDTSL SYISolvent system 90% H2O, 10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.5, Details 1.0 mM BmAsnRS(1-111) U-15N/13C, 20 mM sodium phosphate, 50 mM sodium chloride
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | AsnRS | [U-100% 13C; U-100% 15N] | 1 mM | |
2 | sodium phosphate | natural abundance | 20 mM | |
3 | sodium chloride | natural abundance | 50 mM | |
4 | sodium azide | natural abundance | 0.02 % | |
5 | H2O | natural abundance | 90 % | |
6 | D2O | natural abundance | 10 % |