Kalirin DH1 NMR structure
GPLGSPEFPG RKKEFIMAEL LQTEKAYVRD LHECLETYLW EMTSGVEEIP PGILNKEHII FGNIQEIYDF HNNIFLKELE KYEQLPEDVG HCFVTWADKF QMYVTYCKNK PDSNQLILEH AGTFFDEIQQ RHGLANSISS YLIKPVQRVT KYQLLLKELL TCCEEGKGEL KDGLEVMLSV PKKANDAMHV
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 97.1 % (2246 of 2314) | 96.7 % (1170 of 1210) | 97.2 % (879 of 904) | 98.5 % (197 of 200) |
Backbone | 97.7 % (1096 of 1122) | 97.1 % (372 of 383) | 97.7 % (545 of 558) | 98.9 % (179 of 181) |
Sidechain | 96.4 % (1321 of 1370) | 96.0 % (794 of 827) | 97.1 % (509 of 524) | 94.7 % (18 of 19) |
Aromatic | 97.6 % (201 of 206) | 98.1 % (101 of 103) | 97.0 % (98 of 101) | 100.0 % (2 of 2) |
Methyl | 97.1 % (200 of 206) | 96.1 % (99 of 103) | 98.1 % (101 of 103) |
1. KalDH1
GPLGSPEFPG RKKEFIMAEL LQTEKAYVRD LHECLETYLW EMTSGVEEIP PGILNKEHII FGNIQEIYDF HNNIFLKELE KYEQLPEDVG HCFVTWADKF QMYVTYCKNK PDSNQLILEH AGTFFDEIQQ RHGLANSISS YLIKPVQRVT KYQLLLKELL TCCEEGKGEL KDGLEVMLSV PKKANDAMHVSolvent system 90% H2O/10% D2O, Pressure 1.00 atm, Temperature 298 (±0.5) K, pH 6.80 (±0.05), Details pH 6.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | KalDH1 | [U-100% 13C; U-100% 15N] | 0.6 mM | |
2 | Hepes | natural abundance | 50.0 mM | |
3 | H2O | natural abundance | 90 % | |
4 | D2O | natural abundance | 10 % |
Solvent system 90% H2O/10% D2O, Pressure 1.00 atm, Temperature 298 (±0.5) K, pH 6.80 (±0.05), Details pH 6.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
5 | KalDH1 | [U-100% 15N] | 0.56 mM | |
6 | Hepes | natural abundance | 50.00 mM | |
7 | H2O | natural abundance | 90 % | |
8 | D2O | natural abundance | 10 % |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 97.2 % (4500 of 4628) | 96.8 % (2343 of 2420) | 97.4 % (1761 of 1808) | 99.0 % (396 of 400) |
Backbone | 98.3 % (2206 of 2244) | 97.7 % (748 of 766) | 98.5 % (1099 of 1116) | 99.2 % (359 of 362) |
Sidechain | 96.5 % (2643 of 2740) | 96.2 % (1591 of 1654) | 96.9 % (1015 of 1048) | 97.4 % (37 of 38) |
Aromatic | 94.9 % (391 of 412) | 95.6 % (197 of 206) | 94.1 % (190 of 202) | 100.0 % (4 of 4) |
Methyl | 98.5 % (406 of 412) | 98.1 % (202 of 206) | 99.0 % (204 of 206) |
1. KalDH1
GPLGSPEFPG RKKEFIMAEL LQTEKAYVRD LHECLETYLW EMTSGVEEIP PGILNKEHII FGNIQEIYDF HNNIFLKELE KYEQLPEDVG HCFVTWADKF QMYVTYCKNK PDSNQLILEH AGTFFDEIQQ RHGLANSISS YLIKPVQRVT KYQLLLKELL TCCEEGKGEL KDGLEVMLSV PKKANDAMHVSolvent system 90% H2O/10% D2O, Pressure 1.00 atm, Temperature 298 (±0.5) K, pH 6.80 (±0.05), Details pH 6.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
5 | KalDH1 | [U-100% 15N] | 0.56 mM | |
6 | Hepes | natural abundance | 50.00 mM | |
7 | H2O | natural abundance | 90 % | |
8 | D2O | natural abundance | 10 % |