Solution NMR structure of PAP248-286 in 50% TFE
Polymer type: polypeptide(L)
Total | 1H | |
---|---|---|
All | 85.3 % (226 of 265) | 85.3 % (226 of 265) |
Backbone | 96.2 % (77 of 80) | 96.2 % (77 of 80) |
Sidechain | 80.5 % (149 of 185) | 80.5 % (149 of 185) |
Aromatic | 100.0 % (12 of 12) | 100.0 % (12 of 12) |
Methyl | 90.9 % (20 of 22) | 90.9 % (20 of 22) |
1. entity
GIHKQKEKSR LQGGVLVNEI LNHMKRATQI PSYKKLIMYSolvent system trifluoroethanol/water, Pressure 1 atm, Temperature 298 K, pH 7.5
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | PAP248-286 | natural abundance | 1.2 mM | |
2 | sodium phosphate | natural abundance | 20 mM | |
3 | D2O | [U-99% 2H] | 10 % | |
4 | TFE | [U-99% 2H] | 50 % |