BMRBj - BMREntryMaster

	Total	¹H	¹³C	¹⁵N
All	89.0 % (866 of 973)	89.4 % (457 of 511)	87.6 % (332 of 379)	92.8 % (77 of 83)
Backbone	96.7 % (462 of 478)	97.6 % (161 of 165)	95.3 % (225 of 236)	98.7 % (76 of 77)
Sidechain	83.8 % (477 of 569)	85.5 % (296 of 346)	82.9 % (180 of 217)	16.7 % (1 of 6)
Aromatic	26.7 % (8 of 30)	46.7 % (7 of 15)	0.0 % (0 of 14)	100.0 % (1 of 1)
Methyl	94.4 % (102 of 108)	94.4 % (51 of 54)	94.4 % (51 of 54)

1. UBIQUITIN-LIKE DOMAIN-CONTAINING CTD PHOSPHATASE 1

MALPIIVKWG GQEYSVTTLS EDDTVLDLKQ FLKTLTGVLP ERQKLLGLKV KGKPAENDVK LGALKLKPNT KIMMMGTREE S

Show sample condition

Sample #1

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.0, Details 1.5 MM [U-99% 15N] UBLDOMAIN OF UBLCP1-1, 90% H2O/10% D2O

#	Name	Isotope labeling	Concentration
1	UBIQUITIN-LIKE DOMAIN-CONTAINING CTD PHOSPHATASE 1	[U-99% 15N]	1.5 mM
2	H2O	natural abundance	90 %
3	D2O	natural abundance	10 %

Sample #2

Solvent system 100% D2O, Pressure 1 atm, Temperature 298 K, pH 7.0, Details 1.5 [U-95% 13C

#	Name	Isotope labeling	Type	Concentration
4	UBIQUITIN-LIKE DOMAIN-CONTAINING CTD PHOSPHATASE 1	[U-95% 13C]		1.5 mM
5	D2O	natural abundance		100 %

Sample #3

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.0, Details U-99% 15N/95% 13C] UBLDOMAI OF UBLCP1-2, 90% H2O/10% D2O

#	Name	Isotope labeling	Concentration
6	UBIQUITIN-LIKE DOMAIN-CONTAINING CTD PHOSPHATASE 1	[U-95% 13C; U-95% 15N]	1.5 mM
7	H2O	natural abundance	90 %
8	D2O	natural abundance	10 %

LACS Plot; CA

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	na	indirect	0.2514495
¹H	DSS	methyl protons	internal	direct	1.0
¹⁵N	DSS	methyl protons	na	indirect	0.1013291

Referencing offset: -0.22 ppm, Outliers: 1 Detail

LACS Plot; CB

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	na	indirect	0.2514495
¹H	DSS	methyl protons	internal	direct	1.0
¹⁵N	DSS	methyl protons	na	indirect	0.1013291

Referencing offset: -0.22 ppm, Outliers: 1 Detail

LACS Plot; HA

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	na	indirect	0.2514495
¹H	DSS	methyl protons	internal	direct	1.0
¹⁵N	DSS	methyl protons	na	indirect	0.1013291

Referencing offset: 0.03 ppm, Outliers: 1 Detail

LACS Plot; CO

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	na	indirect	0.2514495
¹H	DSS	methyl protons	internal	direct	1.0
¹⁵N	DSS	methyl protons	na	indirect	0.1013291

Referencing offset: -0.37 ppm, Outliers: 1 Detail

Protein Blocks Logo

Calculated from 20 models in PDB: 2LGD, Strand ID: A Detail

Release date

2012-08-30

Related entities 1. single polypeptide chain, : 1 : 6 : 3 : 1 : 111 entities Detail

Interaction partners 1. single polypeptide chain, : 3 interactors Detail

More details for 3 interactors identified by 2 citations

Experiments performed 9 experiments Detail

1 2D 1H-15N HSQC

Instrument

Bruker DRX - 900 MHz

Sample

State isotropic, Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.0, Details 1.5 MM [U-99% 15N] UBLDOMAIN OF UBLCP1-1, 90% H2O/10% D2O

#	Name	Isotope labeling	Concentration
1	UBIQUITIN-LIKE DOMAIN-CONTAINING CTD PHOSPHATASE 1	[U-99% 15N]	1.5 mM
2	H2O	natural abundance	90 %
3	D2O	natural abundance	10 %

2 3D CBCA(CO)NH