STRUCTURES AND INTERACTIONS ANALYSES OF THE INTEGRIN ALPHA-M BETA-2 CYTOPLASMIC TAILS
Polymer type: polypeptide(L)
Total | 1H | 13C | |
---|---|---|---|
All | 56.0 % (150 of 268) | 79.7 % (126 of 158) | 21.8 % (24 of 110) |
Backbone | 60.7 % (71 of 117) | 95.9 % (47 of 49) | 35.3 % (24 of 68) |
Sidechain | 46.8 % (80 of 171) | 72.5 % (79 of 109) | 1.6 % (1 of 62) |
Aromatic | 42.9 % (12 of 28) | 85.7 % (12 of 14) | 0.0 % (0 of 14) |
Methyl | 50.0 % (3 of 6) | 100.0 % (3 of 3) | 0.0 % (0 of 3) |
1. entity
KLGFFKRQYK DMMSEGGPPG AEPQSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 308 (±2) K, pH 5.6 (±0.01), Details 0.7 mM MYR-ALPHA-M
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | MAC-1 | natural abundance | 0.7 mM | |
2 | deuterated Dodecylphosphocholine | [U-99% 2H] | 200 mM | |
3 | sodium phosphate | natural abundance | 10 mM | |
4 | H2O | natural abundance | 90 % | |
5 | D2O | [U-99% 2H] | 10 % |
Solvent system 100% D2O, Pressure 1 atm, Temperature 308 (±2) K, pH 5.6 (±0.01), Details 0.7 mM MYR-ALPHA-M
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
6 | MAC-1 | natural abundance | 0.7 mM | |
7 | deuterated Dodecylphosphocholine | [U-99% 2H] | 200 mM | |
8 | sodium phosphate | natural abundance | 10 mM | |
9 | D2O | [U-99% 2H] | 100 % |