Solution NMR structure of the d(GGGTTTTGGGTGGGTTTTGGG) quadruplex in sodium conditions.
Polymer type: polydeoxyribonucleotide
Total | 1H | |
---|---|---|
All | 79.8 % (158 of 198) | 79.8 % (158 of 198) |
Suger, PO4 | 87.1 % (128 of 147) | 87.1 % (128 of 147) |
Nucleobase | 58.8 % (30 of 51) | 58.8 % (30 of 51) |
Aromatic | 50.0 % (21 of 42) | 50.0 % (21 of 42) |
Methyl | 100.0 % (9 of 9) | 100.0 % (9 of 9) |
1. DNA
GGGTTTTGGG TGGGTTTTGG GSolvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 293 K, pH 7.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | DNA (5'-D(*GP*GP*GP*TP*TP*TP*TP*GP*GP*GP*TP*GP*GP*GP*TP*TP*TP*TP*GP*GP*G)-3') | natural abundance | 2 mM | |
2 | sodium phosphate | natural abundance | 20 mM | |
3 | H2O | natural abundance | 93 % | |
4 | D2O | [U-100% 2H] | 7 % |
Solvent system 100% D2O, Pressure 1 atm, Temperature 293 K, pH 7.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
5 | DNA (5'-D(*GP*GP*GP*TP*TP*TP*TP*GP*GP*GP*TP*GP*GP*GP*TP*TP*TP*TP*GP*GP*G)-3') | natural abundance | 2 mM | |
6 | sodium phosphate | natural abundance | 20 mM | |
7 | D2O | [U-100% 2H] | 100 % |
Polymer type: polydeoxyribonucleotide
Total | 1H | |
---|---|---|
All | 74.5 % (295 of 396) | 74.5 % (295 of 396) |
Suger, PO4 | 75.2 % (221 of 294) | 75.2 % (221 of 294) |
Nucleobase | 72.5 % (74 of 102) | 72.5 % (74 of 102) |
Aromatic | 66.7 % (56 of 84) | 66.7 % (56 of 84) |
Methyl | 100.0 % (18 of 18) | 100.0 % (18 of 18) |
1. DNA
GGGTTTTGGG TGGGTTTTGG GSolvent system 93% H2O/7% D2O, Pressure 1 atm, Temperature 278 K, pH 7.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | DNA (5'-D(*GP*GP*GP*TP*TP*TP*TP*GP*GP*GP*TP*GP*GP*GP*TP*TP*TP*TP*GP*GP*G)-3') | natural abundance | 2 mM | |
2 | sodium phosphate | natural abundance | 20 mM | |
3 | H2O | natural abundance | 93 % | |
4 | D2O | [U-100% 2H] | 7 % |
Solvent system 100% D2O, Pressure 1 atm, Temperature 278 K, pH 7.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
5 | DNA (5'-D(*GP*GP*GP*TP*TP*TP*TP*GP*GP*GP*TP*GP*GP*GP*TP*TP*TP*TP*GP*GP*G)-3') | natural abundance | 2 mM | |
6 | sodium phosphate | natural abundance | 20 mM | |
7 | D2O | [U-100% 2H] | 100 % |