Solution NMR structure of peptide ImI1 (peak 2)
ID | Type | Value order | Atom ID 1 | Atom ID 2 |
---|---|---|---|---|
1 | disulfide | sing | 1:81S2:SG | 1:CYS8:SG |
2 | disulfide | sing | 1:81S2:SG | 1:CYS12:SG |
Polymer type: polypeptide(L)
Total | 1H | |
---|---|---|
All | 95.0 % (57 of 60) | 95.0 % (57 of 60) |
Backbone | 86.4 % (19 of 22) | 86.4 % (19 of 22) |
Sidechain | 100.0 % (38 of 38) | 100.0 % (38 of 38) |
Aromatic | 100.0 % (6 of 6) | 100.0 % (6 of 6) |
Methyl | 100.0 % (2 of 2) | 100.0 % (2 of 2) |
1. ImI1 (peak 2)
GXASDPRCAW RCXSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 278 K, pH 5.8, Details 1 mM peptide was dissolved in 600 micro liter 100 mM potassium phosphate pH 5.8 buffer.
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | ImI1 (peak 2) | natural abundance | 1 mM | |
2 | potassium phosphate buffer | natural abundance | 100 mM | |
3 | H2O | natural abundance | 90 % | |
4 | D2O | natural abundance | 10 % |