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BMRB: 19952

2MOU

Solution structure of StAR-related lipid transfer domain protein 6 (STARD6)

Authors

Letourneau, D., Bedard, M., Lefebvre, A., LeHoux, J., Lavigne, P.

Assembly

StAR D6

Entity

1. StAR D6 (polymer, Thiol state: all free), 220 monomers, 25021.22 Da Detail

MDFKAIAQQT AQEVLGYNRD TSGWKVVKTS KKITVSSKAS RKFHGNLYRV EGIIPESPAK LSDFLYQTGD RITWDKSLQV YNMVHRIDSD TFICHTITQS FAVGSISPRD FIDLVYIKRY EGNMNIISSK SVDFPEYPPS SNYIRGYNHP CGFVCSPMEE NPAYSKLVMF VQTEMRGKLS PSIIEKTMPS NLVNFILNAK DGIKAHRTPS RRGFHHNSHS

Formula weight

25021.22 Da

Source organism

Homo sapiens

Exptl. method

solution NMR

Refine. method

simulated annealing

Data set

assigned_chemical_shifts, spectral_peak_list

Chem. Shift Complete

Sequence coverage: 98.6 %, Completeness: 86.1 %, Completeness (bb): 96.1 % Detail

Polymer type: polypeptide(L)

	Total	¹H	¹³C	¹⁵N
All	86.1 % (2249 of 2611)	85.0 % (1159 of 1363)	86.7 % (883 of 1019)	90.4 % (207 of 229)
Backbone	96.1 % (1245 of 1296)	96.1 % (423 of 440)	95.5 % (619 of 648)	97.6 % (203 of 208)
Sidechain	79.3 % (1207 of 1523)	79.7 % (736 of 923)	80.7 % (467 of 579)	19.0 % (4 of 21)
Aromatic	30.1 % (74 of 246)	30.9 % (38 of 123)	28.1 % (34 of 121)	100.0 % (2 of 2)
Methyl	98.6 % (207 of 210)	98.1 % (103 of 105)	99.0 % (104 of 105)

1. StAR D6

Show sample condition

Sample

Solvent system 90% H2O/10% D2O, Pressure 1.000 atm, Temperature 298.150 K, pH 7.000

#	Name	Isotope labeling	Type	Concentration
1	StAR_D6	[U-100% 13C; U-100% 15N]		1 mM

LACS Plot; CA

Atom type	Mol. common name	Atom group	Value	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	0.0 ppm	internal	indirect	0.2514495
¹H	water	proton	4.66 ppm	internal	direct	1.0
¹⁵N	DSS	methyl protons	0.0 ppm	internal	indirect	0.1013291

Referencing offset: 0.36 ppm, Outliers: 1 Detail

LACS Plot; CB

Atom type	Mol. common name	Atom group	Value	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	0.0 ppm	internal	indirect	0.2514495
¹H	water	proton	4.66 ppm	internal	direct	1.0
¹⁵N	DSS	methyl protons	0.0 ppm	internal	indirect	0.1013291

Referencing offset: 0.36 ppm, Outliers: 1 Detail

LACS Plot; HA

Atom type	Mol. common name	Atom group	Value	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	0.0 ppm	internal	indirect	0.2514495
¹H	water	proton	4.66 ppm	internal	direct	1.0
¹⁵N	DSS	methyl protons	0.0 ppm	internal	indirect	0.1013291

Referencing offset: -0.01 ppm, Outliers: 3 Detail

LACS Plot; CO

Atom type	Mol. common name	Atom group	Value	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	0.0 ppm	internal	indirect	0.2514495
¹H	water	proton	4.66 ppm	internal	direct	1.0
¹⁵N	DSS	methyl protons	0.0 ppm	internal	indirect	0.1013291

Referencing offset: 0.48 ppm, Outliers: 2 Detail

Protein Blocks Logo

Calculated from 20 models in PDB: 2MOU, Strand ID: A Detail

Release date

2014-05-19

Citation

Solution structure of StAR-related lipid transfer domain protein 6 (STARD6)
Letourneau, D., Bedard, M., Lefebvre, A., LeHoux, J., Lavigne, P.
Not known

Related entities 1. StAR D6, : 1 : 2 : 55 entities Detail

Experiments performed 14 experiments Detail

1 3D HNCACB