BMRB: 25458

NMR structure of an Odin-Sam1 fragment

Authors

Mercurio, F.A., Leone, M.

Assembly

Odin-Sam1 fragment

Entity

1. Odin-Sam1 fragment (polymer, Thiol state: not present), 45 monomers, 4957.565 Da Detail

XSKLLLNGFD DVHFLGSNVM EEQDLRDIGI SDPQHRRKLL QAARX

Formula weight

4957.565 Da

Exptl. method

solution NMR

Refine. method

simulated annealing, torsion angle dynamics

Data set

assigned_chemical_shifts

Chem. Shift Complete

Sequence coverage: 95.6 %, Completeness: 98.5 %, Completeness (bb): 98.9 % Detail

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Polymer type: polypeptide(L)

	Total	1H
All	98.5 % (264 of 268)	98.5 % (264 of 268)
Backbone	98.9 % (87 of 88)	98.9 % (87 of 88)
Sidechain	98.3 % (177 of 180)	98.3 % (177 of 180)
Aromatic	85.7 % (12 of 14)	85.7 % (12 of 14)
Methyl	100.0 % (24 of 24)	100.0 % (24 of 24)

1. entity 1

XSKLLLNGFD DVHFLGSNVM EEQDLRDIGI SDPQHRRKLL QAARX

Show sample condition

Sample

Solvent system trifluoroethanol/water, Pressure 1 atm, Temperature 298 K

#	Name	Isotope labeling	Type	Concentration
1	entity_1	natural abundance		600 uM
2	H2O	natural abundance		30 % v/v
3	2,2,2-trifluoroethanol-d3 (TFE-d3)	[U-99% 2H]		70 % v/v

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Calculated from 20 models in PDB: 2MYQ, Strand ID: A Detail

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Release date

2015-07-12

Citation

Peptide Fragments of Odin-Sam1: Conformational Analysis and Interaction Studies with EphA2-Sam
Mercurio, F.A., Natale, C.DI., Pirone, L., Scognamiglio, P.L., Marasco, D., Pedone, E.M., Saviano, M., Leone, M.
Chembiochem. (2015), 16, 1629-1636, PubMed 26120079 , DOI 10.1002/cbic.201500197 , Abstract

Related entities 1. Odin-Sam1 fragment, : 1 : 3 : 69 entities Detail

Interaction partners 1. Odin-Sam1 fragment, : 6 interactors Detail

Experiments performed 3 experiments Detail