BMRBj - BMREntryMaster

	Total	¹H	¹³C	¹⁵N
All	81.5 % (667 of 818)	79.7 % (345 of 433)	82.1 % (261 of 318)	91.0 % (61 of 67)
Backbone	88.9 % (345 of 388)	90.0 % (117 of 130)	87.2 % (171 of 196)	91.9 % (57 of 62)
Sidechain	77.5 % (383 of 494)	75.2 % (228 of 303)	81.2 % (151 of 186)	80.0 % (4 of 5)
Aromatic	44.8 % (26 of 58)	62.1 % (18 of 29)	25.0 % (7 of 28)	100.0 % (1 of 1)
Methyl	91.7 % (66 of 72)	88.9 % (32 of 36)	94.4 % (34 of 36)

1. entity 1

SAKELRCQCI KTYSKPFHPK FIKELRVIES GPHCANTEII VKLSDGRELC LDPKENWVQR VVEKFL

Show sample condition

Sample #1

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 313 K, pH 7.3, Details 20 mM [U-13C; U-15N] IL-8 1-66, 20 mM HEPES, 90% H2O/10% D2O

#	Name	Isotope labeling	Type	Concentration
1	HEPES	natural abundance		20 mM
2	IL-8 1-66	[U-13C; U-15N]		20 mM

Sample #2

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 313 K, pH 7.3, Details 20 mM [U-15N] IL-8, 20 mM HEPES, 70 mM sodium chloride, 13.5 mg/L Y21M bacteriophage, 90% H2O/10% D2O

#	Name	Isotope labeling	Concentration
3	HEPES	natural abundance	20 mM
4	IL-8	[U-15N]	20 mM
5	Y21M bacteriophage	natural abundance	13.5 mg/L
6	sodium chloride	natural abundance	70 mM

Sample #3

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 313 K, pH 7.3, Details 20 mM [U-15N] IL-8 1-66, 20 mM HEPES, 90% H2O/10% D2O

#	Name	Isotope labeling	Type	Concentration
7	HEPES	natural abundance		20 mM
8	IL-8 1-66	[U-15N]		20 mM

LACS Plot; CA

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	internal	indirect	0.2514495
¹H	DSS	methyl protons	internal	direct	1.0
¹⁵N	DSS	methyl protons	internal	indirect	0.1013291

Referencing offset: -0.62 ppm, Outliers: 1 Detail

LACS Plot; CB

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	internal	indirect	0.2514495
¹H	DSS	methyl protons	internal	direct	1.0
¹⁵N	DSS	methyl protons	internal	indirect	0.1013291

Referencing offset: -0.62 ppm, Outliers: 1 Detail

LACS Plot; HA

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	internal	indirect	0.2514495
¹H	DSS	methyl protons	internal	direct	1.0
¹⁵N	DSS	methyl protons	internal	indirect	0.1013291

Referencing offset: -0.09 ppm, Outliers: 1 Detail

LACS Plot; CO

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	internal	indirect	0.2514495
¹H	DSS	methyl protons	internal	direct	1.0
¹⁵N	DSS	methyl protons	internal	indirect	0.1013291

Referencing offset: 0.26 ppm, Outliers: 1 Detail

Protein Blocks Logo

Calculated from 10 models in PDB: 5WDZ, Strand ID: A Detail

Release date

2017-10-08

Citation 1

Interaction of Monomeric Interleukin-8 with CXCR1 Mapped by Proton-Detected Fast MAS Solid-State NMR
Berkamp, S., Park, S.H., De Angelis, A.A., Marassi, F.M., Opella, S.J.
Biophys. J. (2017), 113, 2695-2705, PubMed 29262362 , DOI 10.1016/j.bpj.2017.09.041 , Abstract

Show more 1 citaion

Citation 2

Structure of monomeric Interleukin-8 and its interactions with the N-terminal Binding Site-I of CXCR1 by solution NMR spectroscopy
Berkamp, S., Park, S.H., Radoicic, J., De Angelis, A.A., Opella, S.J.
J. Biomol. NMR (2017), 69, 111-121, PubMed 29143165 , DOI 10.1007/s10858-017-0128-3 , Abstract

Hide non-primary 1 citaion

Related entities 1. Interleukin-8, : 1 : 12 : 8 : 206 entities Detail

Interaction partners 1. Interleukin-8, : 11 interactors Detail

More details for 11 interactors identified by 6 citations

Experiments performed 7 experiments Detail

1 3D HNCA