HRFLRH peptide NMR structure in the presence of Zn(II)
Polymer type: polypeptide(L)
Total | 1H | 13C | |
---|---|---|---|
All | 92.5 % (74 of 80) | 95.7 % (44 of 46) | 88.2 % (30 of 34) |
Backbone | 80.0 % (24 of 30) | 83.3 % (10 of 12) | 77.8 % (14 of 18) |
Sidechain | 100.0 % (56 of 56) | 100.0 % (34 of 34) | 100.0 % (22 of 22) |
Aromatic | 100.0 % (18 of 18) | 100.0 % (9 of 9) | 100.0 % (9 of 9) |
Methyl | 100.0 % (4 of 4) | 100.0 % (2 of 2) | 100.0 % (2 of 2) |
1. entity 1
HRFLRHXSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 4.2, Details 2 mM [U-13C] hexapeptide HRFLRH, 2 mM Zn(II), 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | HIS-ARG-PHE-LEU-ARG-HIS | [U-13C] | 2 mM | |
2 | Zn(II) | natural abundance | 2 mM |