BMRB: 30566

hGRNA4-28_3s

Authors

Dastpeyman, M., Bansal, P., Wilson, D., Loukas, A., Smout, M., Daly, N.

Assembly

Granulin-4

Entity

1. Granulin-4 (polymer, Thiol state: all disulfide bound), 24 monomers, 2587.950 Da Detail

CDMEVSCPDG YTCCRLQSGA WGCC

Formula weight

2587.95 Da

Entity Connection

disulfide 3 Detail

---

ID	Type	Value order	Atom ID 1	Atom ID 2
1	disulfide	sing	1:CYS1:SG	1:CYS13:SG
2	disulfide	sing	1:CYS7:SG	1:CYS23:SG
3	disulfide	sing	1:CYS14:SG	1:CYS24:SG

Source organism

Homo sapiens

Exptl. method

solution NMR

Refine. method

torsion angle dynamics

Data set

assigned_chemical_shifts, spectral_peak_list

Chem. Shift Complete

Sequence coverage: 95.8 %, Completeness: 91.9 %, Completeness (bb): 96.0 % Detail

Download

• NMR-STAR v3.1 (partial)
• BMRB/XML (partial)
• CSV
• TSV

Polymer type: polypeptide(L)

	Total	1H
All	91.9 % (113 of 123)	91.9 % (113 of 123)
Backbone	96.0 % (48 of 50)	96.0 % (48 of 50)
Sidechain	89.0 % (65 of 73)	89.0 % (65 of 73)
Aromatic	100.0 % (10 of 10)	100.0 % (10 of 10)
Methyl	100.0 % (6 of 6)	100.0 % (6 of 6)

1. entity 1

CDMEVSCPDG YTCCRLQSGA WGCC

Show sample condition

Sample

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 290 K, pH 5, Details 0.5 mM hGRNA4-28_3s, 90% H2O/10% D2O

#	Name	Isotope labeling	Type	Concentration
1	hGRNA4-28_3s	natural abundance		0.5 mM

Hide sample codition

Protein Blocks Logo

Calculated from 20 models in PDB: 6NUG, Strand ID: A Detail

---

Release date

2019-03-20

Related entities 1. Granulin-4, : 1 : 3 : 1 : 77 entities Detail

Interaction partners 1. Granulin-4, : 50 interactors Detail

Experiments performed 2 experiments Detail

Chemical shift validation 3 contents Detail