NMR Solution structure of cyclic tachyplesin I
ID | Type | Value order | Atom ID 1 | Atom ID 2 |
---|---|---|---|---|
1 | disulfide | sing | 1:CYS3:SG | 1:CYS16:SG |
2 | disulfide | sing | 1:CYS7:SG | 1:CYS12:SG |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 81.0 % (187 of 231) | 95.2 % (118 of 124) | 60.2 % (53 of 88) | 84.2 % (16 of 19) |
Backbone | 79.6 % (86 of 108) | 94.7 % (36 of 38) | 67.3 % (35 of 52) | 83.3 % (15 of 18) |
Sidechain | 84.2 % (117 of 139) | 95.3 % (82 of 86) | 65.4 % (34 of 52) | 100.0 % (1 of 1) |
Aromatic | 47.4 % (18 of 38) | 89.5 % (17 of 19) | 0.0 % (0 of 18) | 100.0 % (1 of 1) |
Methyl | 100.0 % (8 of 8) | 100.0 % (4 of 4) | 100.0 % (4 of 4) |
1. entity 1
KWCFRVCYRG ICYRRCRGSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 4, Details 1.0 mg/mL cyclic tachyplesin I, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | cyclic tachyplesin I | natural abundance | 1.0 mg/mL |
Solvent system 100% D2O, Pressure 1 atm, Temperature 298 K, pH 4, Details 1.0 mg/mL cyclic tachyplesin I, 100% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
2 | cyclic tachyplesin I | natural abundance | 1.0 mg/mL |