Solution NMR Structure Of The I24N-delta10-ngMinE Protein From Neisseria gonorrheae
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 29.2 % (301 of 1032) | 18.2 % (99 of 544) | 39.0 % (154 of 395) | 51.6 % (48 of 93) |
Backbone | 57.1 % (288 of 504) | 53.3 % (90 of 169) | 59.3 % (150 of 253) | 58.5 % (48 of 82) |
Sidechain | 10.1 % (62 of 611) | 2.4 % (9 of 375) | 23.6 % (53 of 225) | 0.0 % (0 of 11) |
Aromatic | 0.0 % (0 of 40) | 0.0 % (0 of 20) | 0.0 % (0 of 20) | |
Methyl | 3.8 % (4 of 106) | 3.8 % (2 of 53) | 3.8 % (2 of 53) |
1. entity 1
KQKTATVARD RLQIIIAQER AQEGQTPDYL PTLRKELMEV LSKYVNVSLD NIRISQEKQD GMDVLELNIT LPEQKKVLEH HHHHHSolvent system 95% H2O/5% D2O, Pressure 1 bar, Temperature 298 K, pH 6.5, Details 1 mM U-13C/15N MinE-d30-I24N, 25 mM potassium phosphate, 0.5 mM EDTA, 0.1 mM benzamidine chloride, 95% H2O/5% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | MinE-d30-I24N | [U-13C; U-15N] | 1 mM | |
2 | potassium phosphate | natural abundance | 25 mM | |
3 | EDTA | natural abundance | 0.5 mM | |
4 | benzamidine chloride | natural abundance | 0.1 mM |
Solvent system 90% H2O/10% D2O, Pressure 1 bar, Temperature 298 K, pH 6.5, Details 1 mM 2H/15N MinE-d30-I24N-RDC, 1 mM 2H/15N MinE-d30-I24N-CPMG, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
5 | MinE-d30-I24N-RDC | [U-2H; U-15N] | 1 mM | |
6 | MinE-d30-I24N-CPMG | [U-2H; U-15N] | 1 mM |
Solvent system 95% H2O/5% D2O, Pressure 1 bar, Temperature 298 K, pH 6.5, Details 1 mM U-13C/15N MinE-d30, 25 mM potassium phosphate, 0.5 mM EDTA, 0.1 mM benzamidine chloride, 95% H2O/5% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
7 | MinE-d30 | [U-13C; U-15N] | 1 mM | |
8 | potassium phosphate | natural abundance | 25 mM | |
9 | EDTA | natural abundance | 0.5 mM | |
10 | benzamidine chloride | natural abundance | 0.1 mM |
Solvent system 90% H2O/10% D2O, Pressure 1 bar, Temperature 298 K, pH 6.5, Details 1 mM U-2H/15N MinE-d30-RDC, 1 mM U-2H/15N MinE-d30-CPMG, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
11 | MinE-d30-RDC | [U-2H; U-15N] | 1 mM | |
12 | MinE-d30-CPMG | [U-2H; U-15N] | 1 mM |