Solution NMR structure of the cyclic plant protein PDP-23 in DPC micelles
ID | Type | Value order | Atom ID 1 | Atom ID 2 |
---|---|---|---|---|
1 | disulfide | sing | 1:CYS3:SG | 1:CYS8:SG |
2 | disulfide | sing | 1:CYS14:SG | 1:CYS25:SG |
3 | covalent | sing | 1:GLY1:N | 1:ASP28:C |
Polymer type: polypeptide(L)
Total | 1H | 13C | |
---|---|---|---|
All | 68.1 % (196 of 288) | 98.1 % (158 of 161) | 29.9 % (38 of 127) |
Backbone | 67.6 % (92 of 136) | 100.0 % (55 of 55) | 45.7 % (37 of 81) |
Sidechain | 67.2 % (119 of 177) | 97.2 % (103 of 106) | 22.5 % (16 of 71) |
Aromatic | 48.4 % (31 of 64) | 93.9 % (31 of 33) | 0.0 % (0 of 31) |
Methyl | 58.3 % (7 of 12) | 100.0 % (6 of 6) | 16.7 % (1 of 6) |
1. entity 1
GFCWHHSCVP SGTCADFPWP LGHQCFPDSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 5, Details 2 mg/mL PDP-23, 12 mM DPC, 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | PDP-23 | natural abundance | 2 mg/mL | |
2 | DPC | natural abundance | 12 mM |