BMRB: 30864

D-Phenylseptin - The second residue of PHE of the peptide is a D-amino acid

Authors

Munhoz, V.H.O., Verly, R.M.

Assembly

D-Phenylseptin

Entity

1. D-Phenylseptin (polymer, Thiol state: not present), 18 monomers, 1955.298 Da Detail

FXFDTLKNLA GKVIGALT

Formula weight

1955.298 Da

Source organism

Boana punctata

Exptl. method

solution NMR

Data set

assigned_chemical_shifts, spectral_peak_list

Chem. Shift Complete

Sequence coverage: 94.4 %, Completeness: 62.1 %, Completeness (bb): 72.9 % Detail

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Polymer type: polypeptide(L)

	Total	1H	13C
All	62.1 % (113 of 182)	77.2 % (78 of 101)	43.2 % (35 of 81)
Backbone	72.9 % (62 of 85)	91.7 % (33 of 36)	59.2 % (29 of 49)
Sidechain	56.3 % (63 of 112)	69.2 % (45 of 65)	38.3 % (18 of 47)
Aromatic	20.0 % (4 of 20)	40.0 % (4 of 10)	0.0 % (0 of 10)
Methyl	53.6 % (15 of 28)	78.6 % (11 of 14)	28.6 % (4 of 14)

1. entity 1

FXFDTLKNLA GKVIGALT

Show sample condition

Sample

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.0, Details 2 mM D-Phenylseptin, 200 mM [U-100% 2H] Dodecylphosphocholine, 5 uM DSS, 90% H2O/10% D2O

#	Name	Isotope labeling	Type	Concentration
1	D-Phenylseptin	natural abundance		2 mM
2	Dodecylphosphocholine	[U-100% 2H]		200 mM
3	DSS	natural abundance		5 uM

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Release date

2022-11-20

Citation

NMR structure of D-Phenylseptin in DPC-d38
Munhoz, V.H.O., Verly, R.M.

Related entities 1. D-Phenylseptin, : 1 : 1 entities Detail

Experiments performed 3 experiments Detail