BMRB: 34412

Winter flounder 3 in SDS micelles

Authors

Mason, A.J., Clarke, M.

Assembly

Pleurocidin-like peptide WF3

Entity

1. Pleurocidin-like peptide WF3 (polymer, Thiol state: not present), 24 monomers, 2625.063 Da Detail

FLGALIKGAI HGGRFIHGMI QNHH

Formula weight

2625.063 Da

Source organism

Pseudopleuronectes americanus

Exptl. method

solution NMR

Refine. method

simulated annealing

Data set

assigned_chemical_shifts, spectral_peak_list

Chem. Shift Complete

Sequence coverage: 95.8 %, Completeness: 64.8 %, Completeness (bb): 96.2 % Detail

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Polymer type: polypeptide(L)

	Total	1H
All	64.8 % (94 of 145)	64.8 % (94 of 145)
Backbone	96.2 % (51 of 53)	96.2 % (51 of 53)
Sidechain	46.7 % (43 of 92)	46.7 % (43 of 92)
Aromatic	0.0 % (0 of 18)	0.0 % (0 of 18)
Methyl	35.7 % (5 of 14)	35.7 % (5 of 14)

1. entity 1

FLGALIKGAI HGGRFIHGMI QNHH

Show sample condition

Sample

Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 7.0, Details 0.5 mM NA Peptide, 50 mM U-98% Dodecyl-d25 sulfate sodium salt, SDS-d25 SDS, 0.005 % w/w NA TSP, 90% H2O/10% D2O

#	Name	Isotope labeling	Type	Concentration
1	Peptide	natural abundance		0.5 mM
2	SDS	[U-98% Dodecyl-d25 sulfate sodium salt, SDS-d25]		50 mM
3	TSP	natural abundance		0.005 % w/w

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Protein Blocks Logo

Calculated from 100 models in PDB: 6RZ1, Strand ID: A Detail

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Release date

2020-07-05

Citation

Structure of winter flounder AMP 3
Mason, A.J., Clarke, M.

Related entities 1. Pleurocidin-like peptide WF3, : 1 : 1 : 4 entities Detail

Experiments performed 2 experiments Detail

Chemical shift validation 3 contents Detail