BMRB: 34876

Hybrid-1R G-quadruplex with a +(lpp) loop progression

Authors

Jana, J., Vianney, Y.M., Weisz, K.

Assembly

DNA (27-MER)

Entity

1. DNA (27-MER) (polymer, Thiol state: not present), 27 monomers, 8564.398 Da Detail

GCGTGGGTCA GGGTTGGGTT GGGACGC

Formula weight

8564.398 Da

Source organism

synthetic construct

Exptl. method

solution NMR

Data set

assigned_chemical_shifts

Chemcal Shifts

¹H: 178, ¹³C: 29 assignments Detail

Download

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• BMRB/XML (partial)
• CSV
• TSV

ID	Entity ID	Seq ID	Comp ID	Atom ID	Atom type	Val	Val err	Ambig. code
1	1	1	DG	H1'	H	5.882	0.003	1
2	1	1	DG	H2'	H	2.469	0.004	1
3	1	1	DG	H2''	H	2.650	0.003	1
4	1	1	DG	H3'	H	4.750	0.002	1
5	1	1	DG	H8	H	7.860	0.003	1
6	1	1	DG	C8	C	138.799		1
7	1	2	DC	H1'	H	5.534	0.003	1
8	1	2	DC	H2'	H	1.888	0.002	1
9	1	2	DC	H2''	H	2.216	0.004	1
10	1	2	DC	H3'	H	4.690	0.001	1
11	1	2	DC	H5	H	5.272	0.002	1
12	1	2	DC	H6	H	7.234	0.004	1
13	1	2	DC	H41	H	8.279	0.001	1
14	1	2	DC	H42	H	6.396	0.001	1
15	1	2	DC	C6	C	142.939		1
16	1	3	DG	H1	H	12.792	0.001	1
17	1	3	DG	H1'	H	5.857	0.003	1
18	1	3	DG	H2'	H	2.285	0.002	1
19	1	3	DG	H2''	H	2.492	0.001	1
20	1	3	DG	H3'	H	4.804	0.0	1
21	1	3	DG	H8	H	7.657	0.002	1
22	1	3	DG	C8	C	138.407		1
23	1	4	DT	H1'	H	5.778	0.002	1
24	1	4	DT	H2'	H	1.896	0.002	1
25	1	4	DT	H2''	H	2.738	0.003	1
26	1	4	DT	H3	H	13.392	0.001	1
27	1	4	DT	H3'	H	4.736	0.004	1
28	1	4	DT	H6	H	6.850	0.001	1
29	1	4	DT	H71	H	0.974	0.002	1
30	1	4	DT	H72	H	0.974	0.002	1
31	1	4	DT	H73	H	0.974	0.002	1
32	1	4	DT	C6	C	137.756		1
33	1	5	DG	H1	H	10.941	0.002	1
34	1	5	DG	H1'	H	5.915	0.002	1
35	1	5	DG	H2'	H	3.065	0.001	1
36	1	5	DG	H2''	H	2.739	0.005	1
37	1	5	DG	H3'	H	4.878	0.0	1
38	1	5	DG	H8	H	7.220	0.001	1
39	1	5	DG	C8	C	141.865		1
40	1	6	DG	H1	H	11.194	0.001	1
41	1	6	DG	H1'	H	5.642	0.002	1
42	1	6	DG	H2'	H	2.634	0.001	1
43	1	6	DG	H2''	H	2.462	0.002	1
44	1	6	DG	H3'	H	4.931	0.002	1
45	1	6	DG	H8	H	7.101	0.001	1
46	1	6	DG	C8	C	140.748		1
47	1	7	DG	H1	H	11.339	0.001	1
48	1	7	DG	H1'	H	5.943	0.002	1
49	1	7	DG	H2'	H	2.576	0.003	1
50	1	7	DG	H2''	H	2.539	0.002	1
51	1	7	DG	H3'	H	5.063	0.003	1
52	1	7	DG	H8	H	7.695	0.001	1
53	1	7	DG	C8	C	137.887		1
54	1	8	DT	H1'	H	6.263	0.002	1
55	1	8	DT	H2'	H	2.303	0.002	1
56	1	8	DT	H2''	H	2.504	0.002	1
57	1	8	DT	H3'	H	4.814	0.002	1
58	1	8	DT	H6	H	7.781	0.001	1
59	1	8	DT	H71	H	1.927	0.002	1
60	1	8	DT	H72	H	1.927	0.002	1
61	1	8	DT	H73	H	1.927	0.002	1
62	1	8	DT	C6	C	139.967		1
63	1	9	DC	H1'	H	5.836	0.003	1
64	1	9	DC	H2'	H	1.015	0.004	1
65	1	9	DC	H2''	H	1.849	0.003	1
66	1	9	DC	H3'	H	4.520	0.001	1
67	1	9	DC	H5	H	5.630	0.0	1
68	1	9	DC	H6	H	7.229	0.001	1
69	1	9	DC	C6	C	142.754		1
70	1	10	DA	H1'	H	5.874	0.004	1
71	1	10	DA	H2	H	7.689	0.003	1
72	1	10	DA	H2'	H	2.726	0.001	1
73	1	10	DA	H2''	H	2.668	0.005	1
74	1	10	DA	H3'	H	4.918	0.0	1
75	1	10	DA	H8	H	7.940	0.002	1
76	1	10	DA	C2	C	155.263		1
77	1	10	DA	C8	C	141.266		1
78	1	11	DG	H1	H	11.067	0.001	1
79	1	11	DG	H1'	H	6.066	0.003	1
80	1	11	DG	H2'	H	3.364	0.001	1
81	1	11	DG	H2''	H	2.970	0.002	1
82	1	11	DG	H3'	H	4.903	0.002	1
83	1	11	DG	H8	H	7.447	0.001	1
84	1	11	DG	C8	C	142.337		1
85	1	12	DG	H1	H	11.808	0.002	1
86	1	12	DG	H1'	H	5.967	0.004	1
87	1	12	DG	H2'	H	2.480	0.009	1
88	1	12	DG	H2''	H	2.756	0.001	1
89	1	12	DG	H3'	H	4.990	0.002	1
90	1	12	DG	H8	H	7.870	0.001	1
91	1	12	DG	C8	C	138.222		1
92	1	13	DG	H1	H	10.981	0.001	1
93	1	13	DG	H1'	H	6.266	0.006	1
94	1	13	DG	H2'	H	2.717	0.002	1
95	1	13	DG	H2''	H	2.593	0.0	1
96	1	13	DG	H3'	H	5.023	0.0	1
97	1	13	DG	H8	H	7.742	0.001	1
98	1	13	DG	C8	C	138.237		1
99	1	14	DT	H1'	H	6.595	0.001	1
100	1	14	DT	H2'	H	2.621	0.002	1
101	1	14	DT	H2''	H	2.621	0.002	1
102	1	14	DT	H6	H	7.814	0.002	1
103	1	14	DT	H71	H	2.053	0.001	1
104	1	14	DT	H72	H	2.053	0.001	1
105	1	14	DT	H73	H	2.053	0.001	1
106	1	14	DT	C6	C	140.345		1
107	1	15	DT	H1'	H	6.418	0.002	1
108	1	15	DT	H2'	H	2.381	0.002	2
109	1	15	DT	H2''	H	2.588	0.003	2
110	1	15	DT	H3'	H	4.687	0.001	1
111	1	15	DT	H6	H	7.780	0.001	1
112	1	15	DT	H71	H	1.953	0.0	1
113	1	15	DT	H72	H	1.953	0.0	1
114	1	15	DT	H73	H	1.953	0.0	1
115	1	15	DT	C6	C	140.167		1
116	1	16	DG	H1	H	11.903	0.003	1
117	1	16	DG	H1'	H	6.046	0.002	1
118	1	16	DG	H2'	H	3.179	0.001	1
119	1	16	DG	H2''	H	3.025	0.002	1
120	1	16	DG	H3'	H	4.905	0.002	1
121	1	16	DG	H8	H	7.503	0.001	1
122	1	16	DG	C8	C	142.409		1
123	1	17	DG	H1	H	11.736	0.0	1
124	1	17	DG	H1'	H	5.953	0.006	1
125	1	17	DG	H2'	H	2.510	0.006	1
126	1	17	DG	H2''	H	2.732	0.005	1
127	1	17	DG	H3'	H	5.020	0.004	1
128	1	17	DG	H8	H	7.749	0.002	1
129	1	17	DG	C8	C	138.219		1
130	1	18	DG	H1	H	11.241	0.001	1
131	1	18	DG	H1'	H	6.300	0.002	1
132	1	18	DG	H2'	H	2.692	0.002	1
133	1	18	DG	H2''	H	2.525	0.001	1
134	1	18	DG	H3'	H	5.034	0.002	1
135	1	18	DG	H8	H	7.846	0.002	1
136	1	18	DG	C8	C	138.204		1
137	1	19	DT	H1'	H	6.597	0.001	1
138	1	19	DT	H2'	H	2.621	0.001	1
139	1	19	DT	H2''	H	2.621	0.001	1
140	1	19	DT	H6	H	7.813	0.001	1
141	1	19	DT	H71	H	2.049	0.001	1
142	1	19	DT	H72	H	2.049	0.001	1
143	1	19	DT	H73	H	2.049	0.001	1
144	1	19	DT	C6	C	140.338		1
145	1	20	DT	H1'	H	6.417	0.001	1
146	1	20	DT	H2'	H	2.371	0.002	2
147	1	20	DT	H2''	H	2.587	0.003	2
148	1	20	DT	H3'	H	4.683	0.001	1
149	1	20	DT	H6	H	7.780	0.001	1
150	1	20	DT	H71	H	1.953	0.0	1
151	1	20	DT	H72	H	1.953	0.0	1
152	1	20	DT	H73	H	1.953	0.0	1
153	1	20	DT	C6	C	140.147		1
154	1	21	DG	H1	H	11.723	0.003	1
155	1	21	DG	H1'	H	5.994	0.003	1
156	1	21	DG	H2'	H	3.047	0.001	1
157	1	21	DG	H2''	H	2.967	0.002	1
158	1	21	DG	H3'	H	4.888	0.0	1
159	1	21	DG	H8	H	7.405	0.001	1
160	1	21	DG	C8	C	142.052		1
161	1	22	DG	H1	H	11.826	0.003	1
162	1	22	DG	H1'	H	5.853	0.003	1
163	1	22	DG	H2'	H	2.566	0.006	1
164	1	22	DG	H2''	H	2.796	0.0	1
165	1	22	DG	H3'	H	5.046	0.003	1
166	1	22	DG	H8	H	7.766	0.003	1
167	1	22	DG	C8	C	138.223		1
168	1	23	DG	H1	H	11.089	0.003	1
169	1	23	DG	H1'	H	5.776	0.003	1
170	1	23	DG	H2'	H	2.636	0.005	1
171	1	23	DG	H2''	H	2.656	0.003	1
172	1	23	DG	H3'	H	5.024	0.001	1
173	1	23	DG	H8	H	7.817	0.002	1
174	1	23	DG	C8	C	137.964		1
175	1	24	DA	H1'	H	6.282	0.003	1
176	1	24	DA	H2	H	7.592	0.001	1
177	1	24	DA	H2'	H	2.657	0.01	1
178	1	24	DA	H2''	H	2.871	0.001	1
179	1	24	DA	H3'	H	5.098	0.001	1
180	1	24	DA	H8	H	8.305	0.001	1
181	1	24	DA	C2	C	154.917		1
182	1	24	DA	C8	C	141.278		1
183	1	25	DC	H1'	H	5.570	0.004	1
184	1	25	DC	H2'	H	1.907	0.002	1
185	1	25	DC	H2''	H	2.254	0.003	1
186	1	25	DC	H3'	H	4.830	0.0	1
187	1	25	DC	H5	H	5.237	0.002	1
188	1	25	DC	H6	H	7.223	0.002	1
189	1	25	DC	H41	H	7.983	0.001	1
190	1	25	DC	H42	H	6.357	0.001	1
191	1	25	DC	C6	C	142.548		1
192	1	26	DG	H1	H	12.942	0.004	1
193	1	26	DG	H1'	H	5.878	0.002	1
194	1	26	DG	H2'	H	2.583	0.003	1
195	1	26	DG	H2''	H	2.675	0.005	1
196	1	26	DG	H3'	H	4.930	0.002	1
197	1	26	DG	H8	H	7.843	0.002	1
198	1	26	DG	C8	C	138.209		1
199	1	27	DC	H1'	H	6.134	0.003	1
200	1	27	DC	H2'	H	2.120	0.006	1
201	1	27	DC	H2''	H	2.131	0.006	1
202	1	27	DC	H3'	H	4.451	0.001	1
203	1	27	DC	H5	H	5.503	0.002	1
204	1	27	DC	H6	H	7.427	0.002	1
205	1	27	DC	H41	H	6.652		1
206	1	27	DC	H42	H	8.057		1
207	1	27	DC	C6	C	143.247		1

Release date

2023-12-18

Citation

Impact of loop length and duplex extensions on the design of hybrid-type G-quadruplexes
Jagannath, J., Vianney, Y.M., Weisz, K.
Chem. Commun. (Camb). (2024), 60, 854-857, PubMed 38131370 , DOI 10.1039/d3cc05625b , Abstract

Experiments performed 3 experiments Detail

Chemical shift validation 3 contents Detail