BMRB: 36068

Vaccatide: Antifungal Glutamine-rich 8C-Hevein-like Peptide, vH1

Authors

Xiao, T., Tam, J.P.

Assembly

Vaccatide, vH1

Entity

1. Vaccatide, vH1 (polymer, Thiol state: all disulfide bound), 40 monomers, 4085.547 Da Detail

FQCGRQAGGA RCSNGLCCSQ FGYCGSTPPY CGAGQCQSQC

Formula weight

4085.547 Da

Entity Connection

disulfide 4 Detail

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ID	Type	Value order	Atom ID 1	Atom ID 2
1	disulfide	sing	1:CYS3:SG	1:CYS18:SG
2	disulfide	sing	1:CYS12:SG	1:CYS24:SG
3	disulfide	sing	1:CYS17:SG	1:CYS31:SG
4	disulfide	sing	1:CYS36:SG	1:CYS40:SG

Source organism

Gypsophila vaccaria

Exptl. method

solution NMR

Data set

assigned_chemical_shifts

Chem. Shift Complete

Sequence coverage: 100.0 %, Completeness: 90.6 %, Completeness (bb): 97.7 % Detail

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Polymer type: polypeptide(L)

	Total	1H
All	90.6 % (192 of 212)	90.6 % (192 of 212)
Backbone	97.7 % (84 of 86)	97.7 % (84 of 86)
Sidechain	85.7 % (108 of 126)	85.7 % (108 of 126)
Aromatic	44.4 % (8 of 18)	44.4 % (8 of 18)
Methyl	100.0 % (6 of 6)	100.0 % (6 of 6)

1. Vaccatide, vH1

FQCGRQAGGA RCSNGLCCSQ FGYCGSTPPY CGAGQCQSQC

Show sample condition

Sample

Solvent system 95% H2O/5% D2O, Pressure 1 atm, Temperature 298 K, pH 3.5, Details 1 mM vH1, 55.5 M H2O, 2.92 M [U-100% 2H] D20, 0.1 % TFA, 95% H2O/5% D2O

#	Name	Isotope labeling	Type	Concentration
1	vH1	natural abundance	protein	1 mM
2	TFA	natural abundance		0.1 %
3	H2O	natural abundance	solvent	95 %
4	D20	[U-100% 2H]	solvent	5 %

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Release date

2018-01-17

Citation

Vaccatides: Antifungal Glutamine-Rich Hevein-Like Peptides from Vaccaria hispanica
Wong, K.H., Tan, W.L., Kini, S.G., Xiao, T., Serra, A., Sze, S.K., Tam, J.P.
Front. Plant Sci. (2017), 8, 1100-1100, PubMed 28680440 , DOI 10.3389/fpls.2017.01100 , Abstract

Related entities 1. Vaccatide, vH1, : 1 : 194 entities Detail

Experiments performed 2 experiments Detail