BMRB: 4427

PI7, an orphan peptide isolated from the scorpion Pandinus Imperator: a 1H NMR analysis using a Nano-nmr probe.

Authors

Delepierre, M., Prochnicka-Chalufour, A., Boisbouvier, J., Possani, L.D.

Assembly

toxin 7

Entity

1. toxin 7 (polymer, Thiol state: all disulfide bound), 38 monomers, 4290.968 Da Detail

DEAIRCTGTK DCYIPCRYIT GCFNSRCINK SCKCYGCT

Formula weight

4290.968 Da

Entity Connection

disulfide 4 Detail

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ID	Type	Value order	Atom ID 1	Atom ID 2
1	disulfide	sing	1:CYS6:SG	1:CYS27:SG
2	disulfide	sing	1:CYS12:SG	1:CYS32:SG
3	disulfide	sing	1:CYS16:SG	1:CYS34:SG
4	disulfide	sing	1:CYS22:SG	1:CYS37:SG

Source organism

Pandinus imperator

Exptl. method

NMR

Refine. method

SIMULATED ANNEALING

Data set

assigned_chemical_shifts

Chem. Shift Complete

Sequence coverage: 100.0 %, Completeness: 97.7 %, Completeness (bb): 94.9 % Detail

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Polymer type: polypeptide(L)

	Total	1H
All	97.7 % (214 of 219)	97.7 % (214 of 219)
Backbone	94.9 % (74 of 78)	94.9 % (74 of 78)
Sidechain	99.3 % (140 of 141)	99.3 % (140 of 141)
Aromatic	100.0 % (17 of 17)	100.0 % (17 of 17)
Methyl	100.0 % (13 of 13)	100.0 % (13 of 13)

1. toxin 7

DEAIRCTGTK DCYIPCRYIT GCFNSRCINK SCKCYGCT

Show sample condition

Sample

Pressure 1 atm, Temperature 308 (±1) K

#	Name	Isotope labeling	Type	Concentration
1	toxin 7			1 mM

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Protein Blocks Logo

Calculated from 14 models in PDB: 1QKY, Strand ID: A Detail

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Release date

1999-09-29

Citation

Pi7, an Orphan Peptide from the Scorpion Pandinus imperator: A 1H-NMR Analysis Using a Nano-NMR Probe
Delepierre, M., Prochnicka-Chalufour, A., Boisbouvier, J., Possani, L.D.
Biochemistry (1999), 38, 16756-16765, PubMed , DOI:

Related entities 1. toxin 7, : 1 : 1 : 124 entities Detail

Experiments performed 4 experiments Detail