Solution structure of APAF-1 CARD
MDAKARNCLL QHREALEKDI KTSYIMDHMI SDGFLTISEE EKVRNEPTQQ QRAAMLIKMI LKKDNDSYVS FYNALLHEGY KDLAALLHDG IPVVSSS
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 70.1 % (801 of 1143) | 89.1 % (531 of 596) | 39.9 % (177 of 444) | 90.3 % (93 of 103) |
Backbone | 69.6 % (402 of 578) | 96.9 % (189 of 195) | 42.4 % (122 of 288) | 95.8 % (91 of 95) |
Sidechain | 63.7 % (420 of 659) | 85.3 % (342 of 401) | 30.4 % (76 of 250) | 25.0 % (2 of 8) |
Aromatic | 44.1 % (30 of 68) | 88.2 % (30 of 34) | 0.0 % (0 of 34) | |
Methyl | 93.6 % (103 of 110) | 100.0 % (55 of 55) | 87.3 % (48 of 55) |
1. APOPTOTIC PROTEASE ACTIVATING FACTOR 1
MDAKARNCLL QHREALEKDI KTSYIMDHMI SDGFLTISEE EKVRNEPTQQ QRAAMLIKMI LKKDNDSYVS FYNALLHEGY KDLAALLHDG IPVVSSSPressure 1 atm, Temperature 300 (±1) K, pH 6.5 (±0.2)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | APOPTOTIC PROTEASE ACTIVATING FACTOR 1 | [U-15N] | 0.5 ~ 1.0 mM | |
2 | phosphate buffer | 20 mM | ||
3 | NaCl | 50 mM | ||
4 | DTT | 5 mM |
Pressure 1 atm, Temperature 300 (±1) K, pH 6.5 (±0.2)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
5 | APOPTOTIC PROTEASE ACTIVATING FACTOR 1 | [U-13C] | 1 mM | |
6 | phosphate buffer | 20 mM | ||
7 | NaCl | 50 mM | ||
8 | DTT | 5 mM |
Pressure 1 atm, Temperature 300 (±1) K, pH 6.5 (±0.2)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
9 | APOPTOTIC PROTEASE ACTIVATING FACTOR 1 | 1 mM | ||
10 | phosphate buffer | 20 mM | ||
11 | NaCl | 50 mM | ||
12 | DTT | 5 mM |
Pressure 1 atm, Temperature 300 (±1) K, pH 6.5 (±0.2)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
13 | APOPTOTIC PROTEASE ACTIVATING FACTOR 1 | [U-13C; U-15N; U-80% 2H] | 1 mM | |
14 | phosphate buffer | 20 mM | ||
15 | NaCl | 50 mM | ||
16 | DTT | 5 mM |