Instrument
#1 Model Varian Inova (500 MHz)
#2 Model Varian Inova (750 MHz)
Sample #1
Temperature 298 (±0.1) K, pH 7.50 (±0.02), Details The protein was fully reduced.
| # | Name | Isotope labeling | Type | Concentration |
|---|
| 1 | Plastocyanin from Anabena variabilis | | | 2.9 mM |
|---|
| 2 | COPPER (I) ION | | | 2.9 mM |
|---|
Sample #2
Temperature 298 (±0.1) K, pH 7.50 (±0.02), Details The protein was 18% oxidized with an error of 0.8%.
| # | Name | Isotope labeling | Type | Concentration |
|---|
| 3 | Plastocyanin from Anabena variabilis | | | 2.9 mM |
|---|
| 4 | COPPER (I) ION | | | 2.38 mM |
|---|
| 5 | COPPER (II) ION | | | 0.52 mM |
|---|
Sample #3
Temperature 298 (±0.1) K, pH 7.50 (±0.02), Details The protein was 15.5% oxidized with an error of 0.7%.
| # | Name | Isotope labeling | Type | Concentration |
|---|
| 6 | Plastocyanin from Anabena variabilis | | | 2.9 mM |
|---|
| 7 | COPPER (I) ION | | | 2.45 mM |
|---|
| 8 | COPPER (II) ION | | | 0.45 mM |
|---|
