1H, 13C, and 15N Chemical shift assignments for the third Immunoglobulin domain from the neural cell adhesion molecule, N-CAM
GKDIQVIVNV PPSVRARQST MNATANLSQS VTLACDADGF PEPTMTWTKD GEPIEQEDNE EKYSFNYDGS ELIIKKVDKS DEAEYICIAE NKAGEQDATI HLKVFAK
ID | Type | Value order | Atom ID 1 | Atom ID 2 |
---|---|---|---|---|
1 | disulfide | sing | 0:CYS35:SG | 1:CYS87:SG |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 86.1 % (1044 of 1212) | 95.2 % (600 of 630) | 71.6 % (335 of 468) | 95.6 % (109 of 114) |
Backbone | 81.3 % (514 of 632) | 93.9 % (201 of 214) | 68.4 % (216 of 316) | 95.1 % (97 of 102) |
Sidechain | 92.4 % (630 of 682) | 95.9 % (399 of 416) | 86.2 % (219 of 254) | 100.0 % (12 of 12) |
Aromatic | 41.4 % (29 of 70) | 74.3 % (26 of 35) | 5.9 % (2 of 34) | 100.0 % (1 of 1) |
Methyl | 100.0 % (110 of 110) | 100.0 % (55 of 55) | 100.0 % (55 of 55) |
1. Third Immunoglobulin domain of the Neural cell adhesion molecule
GKDIQVIVNV PPSVRARQST MNATANLSQS VTLACDADGF PEPTMTWTKD GEPIEQEDNE EKYSFNYDGS ELIIKKVDKS DEAEYICIAE NKAGEQDATI HLKVFAKPressure 1 atm, Temperature 298 (±1) K
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Third Immunoglobulin domain of the Neural cell adhesion molecule | [U-15N; U-13C] | 1.0 mM |