BMRBj - BMREntryMaster

	Total	¹H	¹⁵N
All	98.6 % (423 of 429)	98.4 % (361 of 367)	100.0 % (62 of 62)
Backbone	98.9 % (179 of 181)	98.4 % (122 of 124)	100.0 % (57 of 57)
Sidechain	98.4 % (244 of 248)	98.4 % (239 of 243)	100.0 % (5 of 5)
Aromatic	100.0 % (59 of 59)	100.0 % (58 of 58)	100.0 % (1 of 1)
Methyl	100.0 % (16 of 16)	100.0 % (16 of 16)

1. the first fibronectin type II module of human matrix metalloproteinase

RIPVKYGNAD GEYCKFPFLF NGKEYNSCTD TGRSDGFLWC STTYNFEKDG KYGFCPHEAL

Show sample condition

Sample #1

Temperature 298 (±1) K

#	Name	Isotope labeling	Concentration
1	the first fibronectin type II module of human matrix metalloproteinase		0.5 mM
2	H2O		90 %
3	acetone	[U-2H]	10 %

Sample #2

Temperature 298 (±1) K

#	Name	Isotope labeling	Type	Concentration
4	the first fibronectin type II module of human matrix metalloproteinase			0.5 mM

Sample #3

Temperature 298 (±1) K, Details The sample included the tail Leu Phe Thr Met, which wasn't present in the unlabelled sample.

#	Name	Isotope labeling	Type	Concentration
5	the first fibronectin type II module of human matrix metalloproteinase	[U-15N]		0.7 mM

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Calculated from 50 models in PDB: 1KS0, Strand ID: A Detail

Release date

2002-01-20

Citation

The col-1 module of human matrix metalloproteinase-2 (MMP-2): structural/functional relatedness between gelatin-binding fibronectin type II modules and lysine-binding kringle domains
Gehrmann, M., Briknarova, K., Banyai, L., Patthy, L., Llinas, M.
Biol. Chem. (2002), 383, 137-148, PubMed 11928808 , DOI 10.1515/BC.2002.014 , Abstract

Related entities 1. first fibronectin type II module of human matrix metalloproteinase 2, : 1 : 172 entities Detail

Interaction partners 1. first fibronectin type II module of human matrix metalloproteinase 2, : 16 interactors Detail

More details for 16 interactors identified by 10 citations

Experiments performed 8 experiments Detail

1 2D COSY

Instrument

Model Bruker AvanceDMX (500 MHz)

Sample #1

Temperature 298 (±1) K

#	Name	Isotope labeling	Concentration
1	the first fibronectin type II module of human matrix metalloproteinase		0.5 mM
2	H2O		90 %
3	acetone	[U-2H]	10 %

Sample #2

Temperature 298 (±1) K

#	Name	Isotope labeling	Type	Concentration
4	the first fibronectin type II module of human matrix metalloproteinase			0.5 mM

Sample #3

Temperature 298 (±1) K, Details The sample included the tail Leu Phe Thr Met, which wasn't present in the unlabelled sample.

#	Name	Isotope labeling	Type	Concentration
5	the first fibronectin type II module of human matrix metalloproteinase	[U-15N]		0.7 mM

2 2D TOCSY

Instrument

Model Bruker AvanceDMX (500 MHz)

Sample #1

Temperature 298 (±1) K

#	Name	Isotope labeling	Concentration
1	the first fibronectin type II module of human matrix metalloproteinase		0.5 mM
2	H2O		90 %
3	acetone	[U-2H]	10 %

Sample #2

Temperature 298 (±1) K

#	Name	Isotope labeling	Type	Concentration
4	the first fibronectin type II module of human matrix metalloproteinase			0.5 mM

Sample #3

Temperature 298 (±1) K, Details The sample included the tail Leu Phe Thr Met, which wasn't present in the unlabelled sample.

#	Name	Isotope labeling	Type	Concentration
5	the first fibronectin type II module of human matrix metalloproteinase	[U-15N]		0.7 mM

3 2D NOESY

Instrument

Model Bruker AvanceDMX (500 MHz)

Sample #1

Temperature 298 (±1) K

#	Name	Isotope labeling	Concentration
1	the first fibronectin type II module of human matrix metalloproteinase		0.5 mM
2	H2O		90 %
3	acetone	[U-2H]	10 %

Sample #2

Temperature 298 (±1) K

#	Name	Isotope labeling	Type	Concentration
4	the first fibronectin type II module of human matrix metalloproteinase			0.5 mM

Sample #3

Temperature 298 (±1) K, Details The sample included the tail Leu Phe Thr Met, which wasn't present in the unlabelled sample.

#	Name	Isotope labeling	Type	Concentration
5	the first fibronectin type II module of human matrix metalloproteinase	[U-15N]		0.7 mM

4 2D 1H-15N HSQC

Instrument

Model Bruker AvanceDMX (500 MHz)

Sample #1

Temperature 298 (±1) K

#	Name	Isotope labeling	Concentration
1	the first fibronectin type II module of human matrix metalloproteinase		0.5 mM
2	H2O		90 %
3	acetone	[U-2H]	10 %

Sample #2

Temperature 298 (±1) K

#	Name	Isotope labeling	Type	Concentration
4	the first fibronectin type II module of human matrix metalloproteinase			0.5 mM

Sample #3

Temperature 298 (±1) K, Details The sample included the tail Leu Phe Thr Met, which wasn't present in the unlabelled sample.

#	Name	Isotope labeling	Type	Concentration
5	the first fibronectin type II module of human matrix metalloproteinase	[U-15N]		0.7 mM

5 3D HNHA

Instrument

Model Bruker AvanceDMX (500 MHz)

Sample #1

Temperature 298 (±1) K

#	Name	Isotope labeling	Concentration
1	the first fibronectin type II module of human matrix metalloproteinase		0.5 mM
2	H2O		90 %
3	acetone	[U-2H]	10 %

Sample #2

Temperature 298 (±1) K

#	Name	Isotope labeling	Type	Concentration
4	the first fibronectin type II module of human matrix metalloproteinase			0.5 mM

Sample #3

Temperature 298 (±1) K, Details The sample included the tail Leu Phe Thr Met, which wasn't present in the unlabelled sample.

#	Name	Isotope labeling	Type	Concentration
5	the first fibronectin type II module of human matrix metalloproteinase	[U-15N]		0.7 mM

6 3D HNHB

Instrument

Model Bruker AvanceDMX (500 MHz)

Sample #1

Temperature 298 (±1) K

#	Name	Isotope labeling	Concentration
1	the first fibronectin type II module of human matrix metalloproteinase		0.5 mM
2	H2O		90 %
3	acetone	[U-2H]	10 %

Sample #2

Temperature 298 (±1) K

#	Name	Isotope labeling	Type	Concentration
4	the first fibronectin type II module of human matrix metalloproteinase			0.5 mM

Sample #3

Temperature 298 (±1) K, Details The sample included the tail Leu Phe Thr Met, which wasn't present in the unlabelled sample.

#	Name	Isotope labeling	Type	Concentration
5	the first fibronectin type II module of human matrix metalloproteinase	[U-15N]		0.7 mM

7 3D 15N-edited TOCSY

Instrument

Model Bruker AvanceDMX (500 MHz)

Sample #1

Temperature 298 (±1) K

#	Name	Isotope labeling	Concentration
1	the first fibronectin type II module of human matrix metalloproteinase		0.5 mM
2	H2O		90 %
3	acetone	[U-2H]	10 %

Sample #2

Temperature 298 (±1) K

#	Name	Isotope labeling	Type	Concentration
4	the first fibronectin type II module of human matrix metalloproteinase			0.5 mM

Sample #3

Temperature 298 (±1) K, Details The sample included the tail Leu Phe Thr Met, which wasn't present in the unlabelled sample.

#	Name	Isotope labeling	Type	Concentration
5	the first fibronectin type II module of human matrix metalloproteinase	[U-15N]		0.7 mM

8 3D 15N-edited NOESY

Instrument

Model Bruker AvanceDMX (500 MHz)

Sample #1

Temperature 298 (±1) K

#	Name	Isotope labeling	Concentration
1	the first fibronectin type II module of human matrix metalloproteinase		0.5 mM
2	H2O		90 %
3	acetone	[U-2H]	10 %

Sample #2

Temperature 298 (±1) K

#	Name	Isotope labeling	Type	Concentration
4	the first fibronectin type II module of human matrix metalloproteinase			0.5 mM

Sample #3

Temperature 298 (±1) K, Details The sample included the tail Leu Phe Thr Met, which wasn't present in the unlabelled sample.

#	Name	Isotope labeling	Type	Concentration
5	the first fibronectin type II module of human matrix metalloproteinase	[U-15N]		0.7 mM

nullKeywords Fibronectin type II modules, MMP-2 col-gelatin interactionn, kringle-fibronectin type II structural homology

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Found 1 Document (1.875 seconds)

BMRB: 5262

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Related entities 1. first fibronectin type II module of human matrix metalloproteinase 2, : 1 : 172 entities Detail

Interaction partners 1. first fibronectin type II module of human matrix metalloproteinase 2, : 16 interactors Detail

Experiments performed 8 experiments Detail

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