1H, 13C and 15N chemical shift assignments of Schistocerca gregaria chymotrypsin inhibitor
ID | Type | Value order | Atom ID 1 | Atom ID 2 |
---|---|---|---|---|
1 | disulfide | sing | 1:CYS17:SG | 1:CYS28:SG |
2 | disulfide | sing | 1:CYS14:SG | 1:CYS33:SG |
3 | disulfide | sing | 1:CYS4:SG | 1:CYS19:SG |
Polymer type: polypeptide(L)
Total | 1H | 15N | |
---|---|---|---|
All | 88.8 % (198 of 223) | 89.4 % (168 of 188) | 85.7 % (30 of 35) |
Backbone | 93.3 % (97 of 104) | 94.4 % (67 of 71) | 90.9 % (30 of 33) |
Sidechain | 84.9 % (101 of 119) | 86.3 % (101 of 117) | 0.0 % (0 of 2) |
Aromatic | 60.0 % (3 of 5) | 60.0 % (3 of 5) | |
Methyl | 100.0 % (12 of 12) | 100.0 % (12 of 12) |
1. Schistocerca gregaria chymotrypsin inhibitor
EVTCEPGTTF KDKCNTCRCG SDGKSAACTL KACPQTemperature 300 (±1) K, pH 3.0 (±0.2)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Schistocerca gregaria chymotrypsin inhibitor | 2.5 mM |
Temperature 300 (±1) K, pH 3.0 (±0.2)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
2 | Schistocerca gregaria chymotrypsin inhibitor | [U-15N] | 1.5 mM |