BMRB: 5454

NMR solution structure and dynamics of motilin in isotropic phospholipid bicellar solution

Authors

Andersson, A., Maler, L.

Assembly

motilin

Entity

1. motilin (polymer, Thiol state: not present), 22 monomers, 2699.045 Da Detail

FVPIFTYGEL QRMQEKERNK GQ

Formula weight

2699.045 Da

Source organism

Homo sapiens

Exptl. method

NMR

Refine. method

simulated annealing molecular dynamics

Data set

assigned_chemical_shifts

Chem. Shift Complete

Sequence coverage: 100.0 %, Completeness: 79.4 %, Completeness (bb): 95.6 % Detail

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Polymer type: polypeptide(L)

	Total	1H
All	79.4 % (123 of 155)	79.4 % (123 of 155)
Backbone	95.6 % (43 of 45)	95.6 % (43 of 45)
Sidechain	72.7 % (80 of 110)	72.7 % (80 of 110)
Aromatic	42.9 % (6 of 14)	42.9 % (6 of 14)
Methyl	100.0 % (7 of 7)	100.0 % (7 of 7)

1. motilin

FVPIFTYGEL QRMQEKERNK GQ

Show sample condition

Sample

Temperature 310 (±0.5) K, pH 5.5 (±0.2), Details Bicelles were composed of DMPC+DMPG and DHPC in a ratio of the long-chained lipids (DMPC, DMPG) to DHPC of q=0.5. 30% of the long-chained lipids were DMPG. The total amount of lipids was 15 w/v%.

#	Name	Isotope labeling	Type	Concentration
1	motilin			3 mM
2	DMPG			24 mM
3	DMPC			74 mM
4	DHPC			192 mM

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Protein Blocks Logo

Calculated from 24 models in PDB: 1LBJ, Strand ID: A Detail

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Release date

2002-11-05

Citation

NMR solution structure and dynamics of motilin in isotropic phospholipid bicellar solution
Andersson, A., Maler, L.
J. Biomol. NMR (2002), 24, 103-112, PubMed 12495026 , DOI: , Abstract

Entries sharing articles Swiss-Prot: 1 entries Detail

Related entities 1. motilin, : 1 : 4 : 1 : 9 entities Detail

Experiments performed 2 experiments Detail