BMRB: 5598

1H, 13C and 15N backbone resonance assignments of domain 1 of receptor associated protein

Authors

Wang, Y.

Assembly

receptor associated protein-domain 1

Entity

1. receptor associated protein-domain 1 (polymer, Thiol state: not present), 102 monomers, 11902.44 Da Detail

GSYSREKNQP KPSPKRESGE EFRMEKLNQL WEKAQRLHLP PVRLAELHAD LKIQERDELA WKKLKLDGLD EDGEKEARLI RNLNVILAKY GLDGKKDART QV

Formula weight

11902.44 Da

Source organism

Homo sapiens

Exptl. method

NMR

Refine. method

torsiona angle dynamics and simulated anealing

Data set

assigned_chemical_shifts

Chem. Shift Complete

Sequence coverage: 98.0 %, Completeness: 93.6 %, Completeness (bb): 95.7 % Detail

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Polymer type: polypeptide(L)

	Total	1H	13C	15N
All	93.6 % (1176 of 1256)	92.6 % (624 of 674)	95.1 % (451 of 474)	93.5 % (101 of 108)
Backbone	95.7 % (576 of 602)	95.1 % (195 of 205)	96.0 % (288 of 300)	95.9 % (93 of 97)
Sidechain	92.4 % (693 of 750)	91.5 % (429 of 469)	94.8 % (256 of 270)	72.7 % (8 of 11)
Aromatic	100.0 % (58 of 58)	100.0 % (29 of 29)	100.0 % (27 of 27)	100.0 % (2 of 2)
Methyl	95.0 % (95 of 100)	96.0 % (48 of 50)	94.0 % (47 of 50)

1. receptor associated protein, domain 1

GSYSREKNQP KPSPKRESGE EFRMEKLNQL WEKAQRLHLP PVRLAELHAD LKIQERDELA WKKLKLDGLD EDGEKEARLI RNLNVILAKY GLDGKKDART QV

Show sample condition

Sample

Temperature 303 (±0) K, pH 6.5 (±0)

#	Name	Isotope labeling	Type	Concentration
1	receptor associated protein, domain 1			1.2 mM
2	sodium chloride			50 mM

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LACS Plot; CA

Referencing offset: -0.16 ppm, Outliers: 1 Detail

Show chemical shift referencing parameters

Chemical shift reference

Atom type	Mol. common name	Atom group	Value	Ref. method	Ref. type	Shift ratio
13C	DSS	methyl protons	0.0 ppm	null	indirect	0.2514495
1H	DSS	methyl protons	0.0 ppm	internal	direct	1.0
15N	DSS	methyl protons	0.0 ppm	null	indirect	0.1013291

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LACS Plot; CB

Referencing offset: -0.16 ppm, Outliers: 1 Detail

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Chemical shift reference

Atom type	Mol. common name	Atom group	Value	Ref. method	Ref. type	Shift ratio
13C	DSS	methyl protons	0.0 ppm	null	indirect	0.2514495
1H	DSS	methyl protons	0.0 ppm	internal	direct	1.0
15N	DSS	methyl protons	0.0 ppm	null	indirect	0.1013291

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LACS Plot; HA

Referencing offset: 0.05 ppm, Outliers: 1 Detail

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Chemical shift reference

Atom type	Mol. common name	Atom group	Value	Ref. method	Ref. type	Shift ratio
13C	DSS	methyl protons	0.0 ppm	null	indirect	0.2514495
1H	DSS	methyl protons	0.0 ppm	internal	direct	1.0
15N	DSS	methyl protons	0.0 ppm	null	indirect	0.1013291

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LACS Plot; CO

Referencing offset: -0.35 ppm, Outliers: 2 Detail

Show chemical shift referencing parameters

Chemical shift reference

Atom type	Mol. common name	Atom group	Value	Ref. method	Ref. type	Shift ratio
13C	DSS	methyl protons	0.0 ppm	null	indirect	0.2514495
1H	DSS	methyl protons	0.0 ppm	internal	direct	1.0
15N	DSS	methyl protons	0.0 ppm	null	indirect	0.1013291

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Protein Blocks Logo

Calculated from 39 models in PDB: 1OV2, Strand ID: A Detail

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Release date

2003-04-29

Citation

Letter to the Editor: 1H, 13C and 15N resonance assignments of domain 1 of receptor associated protein
Wu, Y., Migliorini, M., Yu, P., Strickland, D.K., Wang, Y.
J. Biomol. NMR (2003), 26, 187-188, PubMed , DOI:

Related entities 1. receptor associated protein-domain 1, : 1 : 4 : 6 entities Detail

Interaction partners 1. receptor associated protein-domain 1, : 17 interactors Detail