BMRB: 5870

Structural Studies of Cu(I)-Bleomycin

Authors

Lehmann, T.E.

Assembly

BLEOMYCIN A2

Entity

1. BLEOMYCIN A2 (non-polymer), 1 monomers, 1416.560 Da
2. CU1 (non-polymer), 63.546 Da

Total weight

1480.1061 Da

Max. entity weight

1416.56 Da

Entity Connection

na 4 Detail

---

ID	Type	Value order	Atom ID 1	Atom ID 2
1	na	sing	2:CU11:CU	1:BLM1:NC
2	na	sing	2:CU11:CU	1:BLM1:NB
3	na	sing	2:CU11:CU	1:BLM1:NG
4	na	sing	2:CU11:CU	1:BLM1:NJ

Source organism

Streptomyces verticillus

Exptl. method

NMR

Data set

assigned_chemical_shifts

Chemcal Shifts

¹H: 70 assignments Detail

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ID	Entity ID	Seq ID	Comp ID	Atom ID	Atom type	Val	Val err	Ambig. code
1	1	1	BLM	HA2	H	7.91		2
2	1	1	BLM	HA1	H	7.18		2
3	1	1	BLM	H2	H	3.98		1
4	1	1	BLM	H3E	H	3.09		2
5	1	1	BLM	H3X	H	2.51		2
6	1	1	BLM	HB1	H	6.81		2
7	1	1	BLM	HB2	H	6.38		2
8	1	1	BLM	HD2	H	7.79		2
9	1	1	BLM	HD1	H	7.00		2
10	1	1	BLM	H5E	H	2.77		2
11	1	1	BLM	H5X	H	2.61		2
12	1	1	BLM	H6	H	4.08		1
13	1	1	BLM	HF2	H	6.77		1
14	1	1	BLM	HF1	H	6.77		1
15	1	1	BLM	HAA	H	1.97		1
16	1	1	BLM	HAB	H	1.97		1
17	1	1	BLM	HAC	H	1.97		1
18	1	1	BLM	H13	H	4.95		1
19	1	1	BLM	H14	H	5.22		1
20	1	1	BLM	H28	H	7.25		1
21	1	1	BLM	H29	H	7.85		1
22	1	1	BLM	HNH	H	9.41		1
23	1	1	BLM	HNK	H	8.23		1
24	1	1	BLM	H34	H	2.37		1
25	1	1	BLM	H31	H	3.77		1
26	1	1	BLM	HBA	H	1.04		1
27	1	1	BLM	HBB	H	1.04		1
28	1	1	BLM	HBC	H	1.04		1
29	1	1	BLM	H33	H	3.68		1
30	1	1	BLM	HCA	H	1.04		1
31	1	1	BLM	HCB	H	1.04		1
32	1	1	BLM	HCC	H	1.04		1
33	1	1	BLM	HNL	H	8.06		1
34	1	1	BLM	H37	H	4.13		1
35	1	1	BLM	H38	H	4.00		1
36	1	1	BLM	HDA	H	1.03		1
37	1	1	BLM	HDB	H	1.03		1
38	1	1	BLM	HDC	H	1.03		1
39	1	1	BLM	HNM	H	8.35		1
40	1	1	BLM	H2E	H	3.17		1
41	1	1	BLM	H2X	H	3.17		1
42	1	1	BLM	H1E	H	3.54		1
43	1	1	BLM	H1X	H	3.54		1
44	1	1	BLM	H44	H	8.11		1
45	1	1	BLM	H47	H	7.88		1
46	1	1	BLM	1H50	H	3.59		1
47	1	1	BLM	2H50	H	3.59		1
48	1	1	BLM	1H51	H	2.15		1
49	1	1	BLM	2H51	H	2.15		1
50	1	1	BLM	1H52	H	3.42		1
51	1	1	BLM	2H52	H	3.42		1
52	1	1	BLM	1H55	H	2.86		1
53	1	1	BLM	2H55	H	2.86		1
54	1	1	BLM	3H55	H	2.86		1
55	1	1	BLM	1H61	H	3.49		2
56	1	1	BLM	2H61	H	3.39		2
57	1	1	BLM	H60	H	3.99		1
58	1	1	BLM	H63	H	5.20		1
59	1	1	BLM	H57	H	3.96		1
60	1	1	BLM	H58	H	4.05		1
61	1	1	BLM	H59	H	3.76		1
62	1	1	BLM	H69	H	3.87		1
63	1	1	BLM	H68	H	4.51		1
64	1	1	BLM	H67	H	3.68		1
65	1	1	BLM	H65	H	3.69		1
66	1	1	BLM	H64	H	4.96		1
67	1	1	BLM	1HNQ	H	6.39		2
68	1	1	BLM	2HNQ	H	6.09		2
69	1	1	BLM	1H66	H	3.86		2
70	1	1	BLM	2H66	H	3.70		2

Release date

2004-10-24

Citation

Structural study of copper(I)-bleomycin
Lehmann, T.E.
J. Biol. Inorg. Chem. (2004), 9, 323-334, PubMed 15015041 , DOI 10.1007/s00775-004-0530-7 , Abstract

Experiments performed 1 experiments Detail