BMRB: 5934

13C and 15N Chemical Shift Assignments for f-MLF-OH

Authors

Rienstra, C.M., Griffin, R.G., Lozano-Perez, T., Tidor, B., McMahon, M.T., Reif, B., Hohwy, M., Tucker-Kellogg, L., Jaroniec, C.P.

Assembly

f-MLF peptide

Entity

1. f-MLF peptide (polymer, Thiol state: not present), 3 monomers, 409.5424 Da Detail

MLF

Formula weight

409.5424 Da

Exptl. method

NMR

Data set

assigned_chemical_shifts

Chem. Shift Complete

Sequence coverage: 100.0 %, Completeness: 86.4 %, Completeness (bb): 100.0 % Detail

Download

• NMR-STAR v3.1 (partial)
• BMRB/XML (partial)
• CSV
• TSV

Polymer type: polypeptide(L)

	Total	13C	15N
All	86.4 % (19 of 22)	84.2 % (16 of 19)	100.0 % (3 of 3)
Backbone	100.0 % (12 of 12)	100.0 % (9 of 9)	100.0 % (3 of 3)
Sidechain	76.9 % (10 of 13)	76.9 % (10 of 13)
Aromatic	40.0 % (2 of 5)	40.0 % (2 of 5)
Methyl	100.0 % (2 of 2)	100.0 % (2 of 2)

1. formyl Methionine-Leucine-Phenylalanine

MLF

Show sample condition

Sample

Temperature 305 (±5) K, Details microcrystals grown by overnight evaporation from 2-Propanol

#	Name	Isotope labeling	Type	Concentration
1	formyl Methionine-Leucine-Phenylalanine

Hide sample codition

Release date

2003-10-15

Citation

De novo determination of peptide structure with solid-state magic-angle spinning NMR spectroscopy
Rienstra, C.M., Griffin, R.G., Lozano-Perez, T., Tidor, B., McMahon, M.T., Reif, B., Hohwy, M., Tucker-Kellogg, L., Jaroniec, C.P.
Proc. Natl. Acad. Sci. U. S. A. (2002), 99, 10260-10265, PubMed 12149447 , DOI 10.1073/pnas.152346599 , Abstract

Experiments performed 2 experiments Detail