BMRB: 6105

Conformational and structural analysis of the equilibrium between single and double-strand beta-helix of a D,L-alternating oligonorleucine

Authors

Navarro, E., Fennude, E., Celda, B.

Assembly

HCO-(D-Nle-L-Nle)3-D-MeNle-L-Nle-D-Nle-L-Nle-OMe

Entity

1. HCO-(D-Nle-L-Nle)3-D-MeNle-L-Nle-D-Nle-L-Nle-OMe (polymer, Thiol state: not present), 10 monomers, 1163.618 × 2 Da

Total weight

2327.236 Da

Max. entity weight

1163.618 Da

Exptl. method

NMR

Data set

assigned_chemical_shifts

Chemcal Shifts

¹H: 60, ¹³C: 10 assignments Detail

Download

• NMR-STAR v3.1 (partial)
• BMRB/XML (partial)
• CSV
• TSV

ID	Entity ID	Seq ID	Comp ID	Atom ID	Atom type	Val	Val err	Ambig. code
1	1	1	DNE	H	H	8.17		1
2	1	1	DNE	HA	H	4.73		1
3	1	1	DNE	HB2	H	1.80		2
4	1	1	DNE	HG2	H	1.78		2
5	1	1	DNE	HD2	H	1.30		2
6	1	1	DNE	HE1	H	0.83		2
7	1	1	DNE	CA	C	52.0		1
8	1	2	NLE	H	H	7.99		1
9	1	2	NLE	HA	H	5.01		1
10	1	2	NLE	HB2	H	1.61		2
11	1	2	NLE	HG2	H	1.51		2
12	1	2	NLE	HD2	H	1.25		2
13	1	2	NLE	HE1	H	0.78		2
14	1	2	NLE	CA	C	50.1		1
15	1	3	DNE	H	H	8.47		1
16	1	3	DNE	HA	H	4.64		1
17	1	3	DNE	HB2	H	1.40		2
18	1	3	DNE	HG2	H	1.63		2
19	1	3	DNE	HD2	H	1.16		2
20	1	3	DNE	HE1	H	0.80		2
21	1	3	DNE	CA	C	51.2		1
22	1	4	NLE	H	H	8.64		1
23	1	4	NLE	HA	H	4.51		1
24	1	4	NLE	HB2	H	1.56		2
25	1	4	NLE	HG2	H	1.64		2
26	1	4	NLE	HD2	H	1.25		2
27	1	4	NLE	HE1	H	0.81		2
28	1	4	NLE	CA	C	51.3		1
29	1	5	DNE	H	H	8.16		1
30	1	5	DNE	HA	H	4.89		1
31	1	5	DNE	HB2	H	1.67		2
32	1	5	DNE	HG2	H	1.67		2
33	1	5	DNE	HD2	H	1.15		2
34	1	5	DNE	HE1	H	0.82		2
35	1	5	DNE	CA	C	52.7		1
36	1	6	NLE	H	H	8.95		1
37	1	6	NLE	HA	H	4.93		1
38	1	6	NLE	HB2	H	1.49		2
39	1	6	NLE	HG2	H	1.49		2
40	1	6	NLE	HD2	H	1.26		2
41	1	6	NLE	HE1	H	0.79		2
42	1	6	NLE	CA	C	47.7		1
43	1	7	DNM	HA	H	5.02		1
44	1	7	DNM	HB2	H	1.87		2
45	1	7	DNM	HG2	H	1.39		2
46	1	7	DNM	HD2	H	1.28		1
47	1	7	DNM	HD3	H	1.14		1
48	1	7	DNM	HE1	H	0.80		2
49	1	7	DNM	CA	C	55.8		1
50	1	8	NLE	H	H	9.29		1
51	1	8	NLE	HA	H	4.38		1
52	1	8	NLE	HB2	H	1.56		2
53	1	8	NLE	HG2	H	1.64		2
54	1	8	NLE	HD2	H	1.22		2
55	1	8	NLE	HE1	H	0.80		2
56	1	8	NLE	CA	C	52.1		1
57	1	9	DNE	H	H	6.64		1
58	1	9	DNE	HA	H	4.71		1
59	1	9	DNE	HB2	H	1.70		2
60	1	9	DNE	HG2	H	1.61		2
61	1	9	DNE	HD2	H	1.29		2
62	1	9	DNE	HE1	H	0.83		2
63	1	9	DNE	CA	C	51.5		1
64	1	10	NLE	H	H	8.64		1
65	1	10	NLE	HA	H	4.43		1
66	1	10	NLE	HB2	H	1.66		2
67	1	10	NLE	HG2	H	1.73		2
68	1	10	NLE	HD2	H	1.27		2
69	1	10	NLE	HE1	H	0.83		2
70	1	10	NLE	CA	C	51.0		1

Release date

2004-05-14

Citation

Conformational and structural analysis of the equilibrium between single- and double-strand beta-helix of a D,L-alternating oligonorleucine
Navarro, E., Fennude, E., Celda, B.
Biopolymers (2004), 73, 229-241, PubMed 14755580 , DOI 10.1002/bip.10549 , Abstract

Experiments performed 3 experiments Detail