1H,15N,13C backbone and sidechain assignment for human ADAP hSH3-1 domain in reduced form
EKKEQKEKEK KEQEIKKKFK LTGPIQVIHL AKACCDVKGG KNELSFKQGE QIEIIRITDN PEGKWLGRTA RGSYGYIKTT AVEIDYDSLK LKKDLE
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 66.6 % (792 of 1190) | 69.7 % (443 of 636) | 58.2 % (263 of 452) | 84.3 % (86 of 102) |
Backbone | 76.4 % (437 of 572) | 85.4 % (169 of 198) | 65.4 % (183 of 280) | 90.4 % (85 of 94) |
Sidechain | 57.8 % (408 of 706) | 62.6 % (274 of 438) | 51.2 % (133 of 260) | 12.5 % (1 of 8) |
Aromatic | 50.0 % (30 of 60) | 50.0 % (15 of 30) | 48.3 % (14 of 29) | 100.0 % (1 of 1) |
Methyl | 77.7 % (73 of 94) | 78.7 % (37 of 47) | 76.6 % (36 of 47) |
1. hSH3-1 domain
EKKEQKEKEK KEQEIKKKFK LTGPIQVIHL AKACCDVKGG KNELSFKQGE QIEIIRITDN PEGKWLGRTA RGSYGYIKTT AVEIDYDSLK LKKDLETemperature 300 (±1) K, pH 7.0 (±0.05)
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | SH3 domain | [U-13C; U-15N] | 1.0 (±0.05) mM | |
2 | NaCl | 20 mM | ||
3 | Potassiumdihydrogenphosphate | 50 mM | ||
4 | Dithtiothreitol | 10 mM |