NMR structure of unliagnded MDM2
MCNTNMSVPT DGAVTTSQIP ASEQETLVRP KPLLLKLLKS VGAQKDTYTM KEVLFYLGQY IMTKRLYDEK QQHIVYCSND LLGDLFGVPS FSVKEHRKIY TMIYRNLVVV NQQESSDSS
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 72.8 % (1032 of 1418) | 77.9 % (575 of 738) | 63.5 % (351 of 553) | 83.5 % (106 of 127) |
Backbone | 74.0 % (521 of 704) | 87.4 % (208 of 238) | 59.4 % (209 of 352) | 91.2 % (104 of 114) |
Sidechain | 73.3 % (607 of 828) | 73.6 % (368 of 500) | 75.2 % (237 of 315) | 15.4 % (2 of 13) |
Aromatic | 48.9 % (46 of 94) | 51.1 % (24 of 47) | 46.8 % (22 of 47) | |
Methyl | 94.3 % (132 of 140) | 97.1 % (68 of 70) | 91.4 % (64 of 70) |
1. Ubiquitin-protein ligase E3 Mdm2 (E.C.6.3.2.-)
MCNTNMSVPT DGAVTTSQIP ASEQETLVRP KPLLLKLLKS VGAQKDTYTM KEVLFYLGQY IMTKRLYDEK QQHIVYCSND LLGDLFGVPS FSVKEHRKIY TMIYRNLVVV NQQESSDSSTemperature 288 K, pH 7.3
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Ubiquitin-protein ligase E3 Mdm2 (E.C.6.3.2.-) | [U-13C; U-15N] | 0.5 mM | |
2 | sodium acetate | [U-2H] | 60 mM | |
3 | phosphate buffer | 60 mM | ||
4 | H2O | 90 % | ||
5 | D2O | 10 % |