BMRB: 6775

1H and Calpha assignments for bombinin H4

Authors

Zangger, K.

Assembly

Bombinin H4

Entity

1. Bombinin H4 (polymer, Thiol state: not present), 20 monomers, 1918.411 Da Detail

IXGPVLGLVG SALGGLLKKI

Formula weight

1918.411 Da

Source organism

Bombina variegata

Exptl. method

NMR

Refine. method

simulated annealing

Data set

assigned_chemical_shifts

Chem. Shift Complete

Sequence coverage: 95.0 %, Completeness: 42.0 %, Completeness (bb): 55.3 % Detail

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Polymer type: polypeptide(L)

	Total	1H	13C
All	42.0 % (81 of 193)	60.2 % (65 of 108)	18.8 % (16 of 85)
Backbone	55.3 % (52 of 94)	85.7 % (36 of 42)	30.8 % (16 of 52)
Sidechain	26.5 % (30 of 113)	43.9 % (29 of 66)	2.1 % (1 of 47)
Methyl	18.4 % (7 of 38)	36.8 % (7 of 19)	0.0 % (0 of 19)

1. Bombinin H4

IXGPVLGLVG SALGGLLKKI

Show sample condition

Sample

Temperature 298 (±1) K, pH 5.0 (±0.2), Details Bombinin H4 in DPC micelles

#	Name	Isotope labeling	Type	Concentration
1	Bombinin H4		protein	3 mM
2	Dodecylphosphocholine (DPC)		lipid	100 mM
3	KPi		buffer	50 mM
4	NaN3		antimicrobial agent	0.02 %

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Protein Blocks Logo

Calculated from 20 models in PDB: 2AP8, Strand ID: A Detail

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Release date

2007-03-26

Citation

Structures of the glycine-rich diastereomeric peptides bombinin H2 and H4
Zangger, K., Gossler, R., Khatai, L., Lohner, K., Jilek, A.
Toxicon. (2008), 52, 246-254, PubMed 18586045 , DOI 10.1016/j.toxicon.2008.05.011 , Abstract

Related entities 1. Bombinin H4, : 1 : 5 : 49 entities Detail

Experiments performed 3 experiments Detail