BMRBj - BMREntryMaster

	Total	¹H	¹³C	¹⁵N
All	63.1 % (841 of 1332)	68.3 % (474 of 694)	53.9 % (280 of 519)	73.1 % (87 of 119)
Backbone	66.4 % (442 of 666)	78.7 % (181 of 230)	53.2 % (174 of 327)	79.8 % (87 of 109)
Sidechain	62.5 % (481 of 769)	63.1 % (293 of 464)	63.7 % (188 of 295)	0.0 % (0 of 10)
Aromatic	18.6 % (22 of 118)	35.6 % (21 of 59)	1.7 % (1 of 59)
Methyl	83.0 % (93 of 112)	80.4 % (45 of 56)	85.7 % (48 of 56)

1. TA0895

MGTSHHHHHH SSGRENLYFQ SHMVTVRYYA TLRPITKKKE ETFNGISKIS ELLERLKVEY GSEFTKQMYD GNNLFKNVII LVNGNNITSM KGLDTEIKDD DKIDLFPPVA GG

Show sample condition

Sample #1

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
1	TA0895	[U-90% 15N]	protein	1.5 mM

Sample #2

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
2	TA0895	[U-98% 13C]	protein	1.2 mM

Sample #3

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
3	TA0895	[U-90% 15N; U-98% 13C]	protein	1.5 mM

LACS Plot; CA

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	external	indirect	0.2514495
¹H	DSS	methyl protons	internal	direct	1.0
¹⁵N	DSS	methyl protons	external	indirect	0.1013291

Referencing offset: -0.73 ppm, Outliers: 5 Detail

LACS Plot; CB

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	external	indirect	0.2514495
¹H	DSS	methyl protons	internal	direct	1.0
¹⁵N	DSS	methyl protons	external	indirect	0.1013291

Referencing offset: -0.73 ppm, Outliers: 5 Detail

LACS Plot; HA

Atom type	Mol. common name	Atom group	Ref. method	Ref. type	Shift ratio
¹³C	DSS	methyl protons	external	indirect	0.2514495
¹H	DSS	methyl protons	internal	direct	1.0
¹⁵N	DSS	methyl protons	external	indirect	0.1013291

Referencing offset: 0.06 ppm, Outliers: 2 Detail

Protein Blocks Logo

Calculated from 20 models in PDB: 2G1E, Strand ID: A Detail

Release date

2006-11-05

Citation

Solution structure of TA0895, a MoaD homologue from Thermoplasma acidophilum
Jung, J., Yeo, I., Hong, E., Yee, A., Arrowsmith, C.H., Lee, W.
Proteins (2006), 65, 1055-1057, PubMed 17019685 , DOI 10.1002/prot.21171 , Abstract

Related entities 1. TA0895, : 1 : 1 : 8 entities Detail

Experiments performed 7 experiments Detail

1 1H15N HSQC

Instrument

#1 Model Bruker DRX500 (500 MHz)

#2 Model Bruker DRX600 (600 MHz) Details DRX600 with cryoprobe

#3 Model Varian INOVA (600 MHz)

Sample #1

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
1	TA0895	[U-90% 15N]	protein	1.5 mM

Sample #2

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
2	TA0895	[U-98% 13C]	protein	1.2 mM

Sample #3

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
3	TA0895	[U-90% 15N; U-98% 13C]	protein	1.5 mM

2 HNCACB

Instrument

#1 Model Bruker DRX500 (500 MHz)

#2 Model Bruker DRX600 (600 MHz) Details DRX600 with cryoprobe

#3 Model Varian INOVA (600 MHz)

Sample #1

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
1	TA0895	[U-90% 15N]	protein	1.5 mM

Sample #2

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
2	TA0895	[U-98% 13C]	protein	1.2 mM

Sample #3

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
3	TA0895	[U-90% 15N; U-98% 13C]	protein	1.5 mM

3 CBCA(CO)NH

Instrument

#1 Model Bruker DRX500 (500 MHz)

#2 Model Bruker DRX600 (600 MHz) Details DRX600 with cryoprobe

#3 Model Varian INOVA (600 MHz)

Sample #1

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
1	TA0895	[U-90% 15N]	protein	1.5 mM

Sample #2

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
2	TA0895	[U-98% 13C]	protein	1.2 mM

Sample #3

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
3	TA0895	[U-90% 15N; U-98% 13C]	protein	1.5 mM

4 HNCA

Instrument

#1 Model Bruker DRX500 (500 MHz)

#2 Model Bruker DRX600 (600 MHz) Details DRX600 with cryoprobe

#3 Model Varian INOVA (600 MHz)

Sample #1

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
1	TA0895	[U-90% 15N]	protein	1.5 mM

Sample #2

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
2	TA0895	[U-98% 13C]	protein	1.2 mM

Sample #3

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
3	TA0895	[U-90% 15N; U-98% 13C]	protein	1.5 mM

5 HNHA

Instrument

#1 Model Bruker DRX500 (500 MHz)

#2 Model Bruker DRX600 (600 MHz) Details DRX600 with cryoprobe

#3 Model Varian INOVA (600 MHz)

Sample #1

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
1	TA0895	[U-90% 15N]	protein	1.5 mM

Sample #2

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
2	TA0895	[U-98% 13C]	protein	1.2 mM

Sample #3

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
3	TA0895	[U-90% 15N; U-98% 13C]	protein	1.5 mM

6 C(CCCO)NH

Instrument

#1 Model Bruker DRX500 (500 MHz)

#2 Model Bruker DRX600 (600 MHz) Details DRX600 with cryoprobe

#3 Model Varian INOVA (600 MHz)

Sample #1

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
1	TA0895	[U-90% 15N]	protein	1.5 mM

Sample #2

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
2	TA0895	[U-98% 13C]	protein	1.2 mM

Sample #3

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
3	TA0895	[U-90% 15N; U-98% 13C]	protein	1.5 mM

7 HCCH-TOCSY

Instrument

#1 Model Bruker DRX500 (500 MHz)

#2 Model Bruker DRX600 (600 MHz) Details DRX600 with cryoprobe

#3 Model Varian INOVA (600 MHz)

Sample #1

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
1	TA0895	[U-90% 15N]	protein	1.5 mM

Sample #2

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
2	TA0895	[U-98% 13C]	protein	1.2 mM

Sample #3

Temperature 298 (±0.1) K, pH 7.4 (±0.1)

#	Name	Isotope labeling	Type	Concentration
3	TA0895	[U-90% 15N; U-98% 13C]	protein	1.5 mM

nullKeywords MoaD, molybdopterin

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Found 1 Document (1.577 seconds)

BMRB: 6982

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Chemical shift reference

Chemical shift reference

Chemical shift reference

Related entities 1. TA0895, : 1 : 1 : 8 entities Detail

Experiments performed 7 experiments Detail

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