Solution structure of 55-72 segment of staphylococcal nuclease
Polymer type: polypeptide(L)
Total | 1H | 13C | |
---|---|---|---|
All | 77.9 % (152 of 195) | 84.1 % (95 of 113) | 69.5 % (57 of 82) |
Backbone | 78.7 % (70 of 89) | 97.2 % (35 of 36) | 66.0 % (35 of 53) |
Sidechain | 80.5 % (99 of 123) | 77.9 % (60 of 77) | 84.8 % (39 of 46) |
Aromatic | 30.0 % (3 of 10) | 60.0 % (3 of 5) | 0.0 % (0 of 5) |
Methyl | 87.5 % (14 of 16) | 87.5 % (7 of 8) | 87.5 % (7 of 8) |
1. 18-mer peptide from Thermonuclease (E.C.3.1.31.1)
GPEASAFTKK MVENAKKIPressure 1 atm, Temperature 298 K, pH 5.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | 18-mer peptide from Thermonuclease (E.C.3.1.31.1) | 2.0 mM | ||
2 | DSS | 0.02 mM | ||
3 | NaN3 | 0.01 mM | ||
4 | trifluoroethanol-d4 | 40 % | ||
5 | H2O | 60 % |