BMRB: 7389

sPLA2 inhibitor 9

Authors

Thwin, M.M., Satyanarayanajois, D.S., Nagarajarao, L.M., Sato, K., Gopalakrishnakone, P.P., Arjunan, P.

Assembly

pip9

Entity

1. pip9 (polymer, Thiol state: not present), 9 monomers, 1039.141 Da Detail

VDIHVWDGV

Formula weight

1039.141 Da

Exptl. method

solution NMR

Refine. method

TORSION ANGLE DYNAMICS

Data set

assigned_chemical_shifts

Chem. Shift Complete

Sequence coverage: 100.0 %, Completeness: 81.6 %, Completeness (bb): 100.0 % Detail

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Polymer type: polypeptide(L)

	Total	1H
All	81.6 % (40 of 49)	81.6 % (40 of 49)
Backbone	100.0 % (19 of 19)	100.0 % (19 of 19)
Sidechain	70.0 % (21 of 30)	70.0 % (21 of 30)
Aromatic	37.5 % (3 of 8)	37.5 % (3 of 8)
Methyl	62.5 % (5 of 8)	62.5 % (5 of 8)

1. pip9

VDIHVWDGV

Show sample condition

Sample

Solvent system DMSO, Pressure 1 atm, Details DMSO

#	Name	Isotope labeling	Type	Concentration
1	pip9	natural abundance		4.5 mM
2	Dimethyl sulfoxide	natural abundance		50 %
3	H2O	natural abundance		50 %

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Protein Blocks Logo

Calculated from 20 models in PDB: 2P5H, Strand ID: A Detail

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Release date

2008-02-19

Citation

Novel peptide inhibitors of human secretory phospholipase A2 with antiinflammatory activity: solution structure and molecular modeling
Thwin, M.M., Satyanarayanajois, D.S., Nagarajarao, L.M., Sato, K., Arjunan, P., Ramapatna, S.L., Kumna, P.V., Gopalakrishnakone, P.P.
J. Med. Chem. (2007), 50, 5938-5950, PubMed 17973469 , DOI 10.1021/jm070385x , Abstract

Entries sharing articles BMRB: 2 entries Detail

Related entities 1. pip9, : 1 entities Detail

Experiments performed 1 experiments Detail