BMRB: 11021

NMR STRUCTURE OF THE MUTANT OF CHIGNOLIN, CLN025

Authors

KATO, Y., ISHIMURA, M., HONDA, S.

Assembly

CLN025

Entity

1. CLN025 (polymer, Thiol state: not present), 10 monomers, 1294.321 Da Detail

YYDPETGTWY

Formula weight

1294.321 Da

Exptl. method

solution NMR

Data set

assigned_chemical_shifts

Chem. Shift Complete

Sequence coverage: 100.0 %, Completeness: 83.9 %, Completeness (bb): 100.0 % Detail

Download

• NMR-STAR v3.1 (partial)
• BMRB/XML (partial)
• CSV
• TSV

Polymer type: polypeptide(L)

	Total	1H
All	83.9 % (52 of 62)	83.9 % (52 of 62)
Backbone	100.0 % (20 of 20)	100.0 % (20 of 20)
Sidechain	76.2 % (32 of 42)	76.2 % (32 of 42)
Aromatic	66.7 % (12 of 18)	66.7 % (12 of 18)
Methyl	100.0 % (2 of 2)	100.0 % (2 of 2)

1. CLN025

YYDPETGTWY

Show sample condition

Sample

Solvent system 95% H2O/5% D2O, Pressure 1 atm, Temperature 298 K, pH 5.7

#	Name	Isotope labeling	Type	Concentration
1	CLN025	natural abundance		2 mM
2	sodium phosphate	natural abundance		20 mM
3	sodium azide	natural abundance		0.02 %
4	DSS	natural abundance		0.01 %
5	H2O			95 %
6	D2O			5 %

Hide sample codition

Release date

2008-11-10

Citation 1

Crystal structure of a ten-amino acid protein
HONDA, S., AKIBA, T., KATO, Y.S., SAWADA, Y., SEKIJIMA, M., ISHIMURA, M., OOISHI, A., WATANABE, H., ODAHARA, T., HARATA, K.
J. Am. Chem. Soc. (2008), 130, 15327-15331, PubMed 18950166 , DOI 10.1021/ja8030533 , Abstract

Show more 1 citaion

Citation 2

10 residue folded peptide designed by segment statistics
HONDA, S., YAMASAKI, K., SAWADA, Y., MORII, H.
Structure (2004), 12, 1507-1518, PubMed 15296744 , DOI 10.1016/j.str.2004.05.022 , Abstract

Hide non-primary 1 citaion

Entries sharing articles BMRB: 3 entries Detail

Related entities 1. CLN025, : 1 : 1 : 2 : 1 entities Detail

Experiments performed 3 experiments Detail

Chemical shift validation 3 contents Detail