Backbone chemical shift assignements for monomeric apoSOD1 - variant A4V
ATKVVAVLKG DGPVQGIINF EQKESNGPVK VWGSIKGLTE GLHGFHVHEE EDNTAGCTSA GPHFNPLSRK HGGPKDEERH VGDLGNVTAD KDGVADVSIE DSVISLSGDH AIIGRTLVVH EKADDLGKGG NEESTKTGNA GSRLACGVIG IAQ
ID | Type | Value order | Atom ID 1 | Atom ID 2 |
---|---|---|---|---|
1 | disulfide | sing | 1:CYS57:SG | 1:CYS146:SG |
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 46.5 % (755 of 1622) | 24.5 % (204 of 834) | 66.5 % (418 of 629) | 83.6 % (133 of 159) |
Backbone | 75.9 % (689 of 908) | 47.1 % (153 of 325) | 92.6 % (403 of 435) | 89.9 % (133 of 148) |
Sidechain | 21.7 % (183 of 843) | 10.2 % (52 of 509) | 40.6 % (131 of 323) | 0.0 % (0 of 11) |
Aromatic | 0.0 % (0 of 74) | 0.0 % (0 of 37) | 0.0 % (0 of 36) | 0.0 % (0 of 1) |
Methyl | 15.9 % (27 of 170) | 12.9 % (11 of 85) | 18.8 % (16 of 85) |
1. SOD1
ATKVVAVLKG DGPVQGIINF EQKESNGPVK VWGSIKGLTE GLHGFHVHEE EDNTAGCTSA GPHFNPLSRK HGGPKDEERH VGDLGNVTAD KDGVADVSIE DSVISLSGDH AIIGRTLVVH EKADDLGKGG NEESTKTGNA GSRLACGVIG IAQSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.3
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | SOD1 | [U-100% 13C; U-100% 15N] | 1 mM | |
2 | MES | natural abundance | 10 mM | |
3 | EDTA | natural abundance | 1 mM | |
4 | D2O | natural abundance | 10 % |