Backbone and sidechain 1H, 15N and 13C assignments of the NLRP7 Pyrin domain
GHMTSPQLEW TLQTLLEQLN EDELKSFKSL LWAFPLEDVL QKTPWSEVEE ADGKKLAEIL VNTSSENWIR NATVNILEEM NLTELCKMAK AEMMEDGQLE HHHHHH
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 87.9 % (1114 of 1268) | 90.3 % (595 of 659) | 85.1 % (418 of 491) | 85.6 % (101 of 118) |
Backbone | 91.0 % (573 of 630) | 90.1 % (191 of 212) | 92.4 % (291 of 315) | 88.3 % (91 of 103) |
Sidechain | 86.0 % (637 of 741) | 90.4 % (404 of 447) | 79.9 % (223 of 279) | 66.7 % (10 of 15) |
Aromatic | 28.1 % (27 of 96) | 56.3 % (27 of 48) | 0.0 % (0 of 44) | 0.0 % (0 of 4) |
Methyl | 100.0 % (118 of 118) | 100.0 % (59 of 59) | 100.0 % (59 of 59) |
1. NLRP7 Pyd
GHMTSPQLEW TLQTLLEQLN EDELKSFKSL LWAFPLEDVL QKTPWSEVEE ADGKKLAEIL VNTSSENWIR NATVNILEEM NLTELCKMAK AEMMEDGQLE HHHHHHSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | NLRP7 Pyd | [U-100% 15N] | 1.0 mM | |
2 | sodium phosphate | natural abundance | 20 mM | |
3 | sodium chloride | natural abundance | 50 mM | |
4 | TCEP | natural abundance | 0.25 mM | |
5 | H2O | natural abundance | 90 % | |
6 | D2O | natural abundance | 10 % |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
7 | NLRP7 Pyd | [U-100% 13C; U-100% 15N] | 1.0 mM | |
8 | sodium phosphate | natural abundance | 20 mM | |
9 | sodium chloride | natural abundance | 50 mM | |
10 | TCEP | natural abundance | 0.25 mM | |
11 | H2O | natural abundance | 90 % | |
12 | D2O | natural abundance | 10 % |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
13 | NLRP7 Pyd | natural abundance | 1.0 mM | |
14 | sodium phosphate | natural abundance | 20 mM | |
15 | sodium chloride | natural abundance | 50 mM | |
16 | TCEP | natural abundance | 0.25 mM | |
17 | H2O | natural abundance | 90 % | |
18 | D2O | natural abundance | 10 % |