Chemical shift assignments of CaBP1 with 3 Ca2+ bound
MGNCVKYPLR NLSRKDRSLR PEEIEELREA FREFDKDKDG YINCRDLGNC MRTMGYMPTE MELIELSQQI NMNLGGHVDF DDFVELMGPK LLAETADMIG VKELRDAFRE FDTNGDGEIS TSELREAMRK LLGHQVGHRD IEEIIRDVDL NGDGRVDFEE FVRMMSR
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 65.4 % (1277 of 1953) | 61.5 % (633 of 1030) | 67.2 % (503 of 749) | 81.0 % (141 of 174) |
Backbone | 85.7 % (852 of 994) | 84.9 % (292 of 344) | 86.2 % (420 of 487) | 85.9 % (140 of 163) |
Sidechain | 50.4 % (560 of 1112) | 49.7 % (341 of 686) | 52.5 % (218 of 415) | 9.1 % (1 of 11) |
Aromatic | 31.9 % (37 of 116) | 63.8 % (37 of 58) | 0.0 % (0 of 58) | |
Methyl | 81.6 % (124 of 152) | 81.6 % (62 of 76) | 81.6 % (62 of 76) |
1. CaBP1
MGNCVKYPLR NLSRKDRSLR PEEIEELREA FREFDKDKDG YINCRDLGNC MRTMGYMPTE MELIELSQQI NMNLGGHVDF DDFVELMGPK LLAETADMIG VKELRDAFRE FDTNGDGEIS TSELREAMRK LLGHQVGHRD IEEIIRDVDL NGDGRVDFEE FVRMMSRSolvent system 95% H2O/5% D2O, Pressure 1 atm, Temperature 310 K, pH 7.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | CaBP1 | [U-98% 13C; U-98% 15N] | 1.0 mM | |
2 | calcium | natural abundance | 5.0 mM | |
3 | TRIS | natural abundance | 10.0 mM | |
4 | H2O | natural abundance | 95 % | |
5 | D2O | natural abundance | 5 % |