The Structure of RNA Internal Loops with Tandem AG Pairs: 5'UAGA/3'AGAU
Polymer type: polyribonucleotide
Total | 1H | 13C | 15N | 31P | |
---|---|---|---|---|---|
All | 72.8 % (134 of 184) | 95.7 % (90 of 94) | 39.2 % (29 of 74) | 100.0 % (5 of 5) | 90.9 % (10 of 11) |
Suger, PO4 | 63.6 % (84 of 132) | 97.0 % (64 of 66) | 18.2 % (10 of 55) | 90.9 % (10 of 11) | |
Nucleobase | 96.2 % (50 of 52) | 92.9 % (26 of 28) | 100.0 % (19 of 19) | 100.0 % (5 of 5) | |
Aromatic | 100.0 % (48 of 48) | 100.0 % (24 of 24) | 100.0 % (19 of 19) | 100.0 % (5 of 5) |
1. RNA (5'-R(*GP*AP*CP*UP*AP*GP*AP*GP*UP*CP*A)-3')
GACUAGAGUC ASolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 288 K, pH 6.1
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | RNA (5'-R(*GP*AP*CP*UP*AP*GP*AP*GP*UP*CP*A)-3') | natural abundance | 1 mM | |
2 | sodium chloride | natural abundance | 80 mM | |
3 | sodium phosphate | natural abundance | 10 mM | |
4 | EDTA | natural abundance | 0.5 mM | |
5 | H2O | natural abundance | 90 % | |
6 | D2O | natural abundance | 10 % |
Solvent system 100% D2O, Pressure 1 atm, Temperature 288 K, pH 6.1
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
7 | RNA (5'-R(*GP*AP*CP*UP*AP*GP*AP*GP*UP*CP*A)-3') | natural abundance | 1 mM | |
8 | sodium chloride | natural abundance | 80 mM | |
9 | sodium phosphate | natural abundance | 10 mM | |
10 | EDTA | natural abundance | 0.5 mM | |
11 | D2O | natural abundance | 100 % |