Solution NMR Structure of protein STY4237 (residues 36-120) from Salmonella enterica, Northeast Structural Genomics Consortium Target SlR115
MAPLQQKQVV VSNKREKPVN DRRSRQQEVS PAGTSMRYEA SFKPLNGGLE KTFRLQAQQY HALTVGDQGT LSYKGTRFVG FVSRTPDNEL EHHHHHH
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 86.3 % (988 of 1145) | 83.1 % (502 of 604) | 89.0 % (388 of 436) | 93.3 % (98 of 105) |
Backbone | 93.0 % (532 of 572) | 90.8 % (178 of 196) | 94.0 % (267 of 284) | 94.6 % (87 of 92) |
Sidechain | 81.7 % (542 of 663) | 79.4 % (324 of 408) | 85.5 % (207 of 242) | 84.6 % (11 of 13) |
Aromatic | 41.3 % (38 of 92) | 43.5 % (20 of 46) | 39.1 % (18 of 46) | |
Methyl | 98.8 % (81 of 82) | 97.6 % (40 of 41) | 100.0 % (41 of 41) |
1. SlR115
MAPLQQKQVV VSNKREKPVN DRRSRQQEVS PAGTSMRYEA SFKPLNGGLE KTFRLQAQQY HALTVGDQGT LSYKGTRFVG FVSRTPDNEL EHHHHHHSolvent system 95% H2O/5% D2O, Pressure 1 atm, Temperature 293 K, pH 6.5, Details 1.1 mM [U-100% 13C; U-100% 15N] SlR115, 95% H2O/5% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | SlR115 | [U-100% 13C; U-100% 15N] | 1.1 mM | |
2 | NaCl | natural abundance | 100 mM | |
3 | MES | natural abundance | 20 mM | |
4 | CaCl2 | natural abundance | 5 mM | |
5 | NaN3 | natural abundance | 0.05 % | |
6 | DTT | natural abundance | 10 mM | |
7 | H2O | natural abundance | 95 % | |
8 | D2O | natural abundance | 5 % |
Solvent system 100% D2O, Pressure 1 atm, Temperature 293 K, pH 6.5, Details 1.1 mM [U-100% 13C; U-100% 15N] SlR115, 100% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
9 | SlR115 | [U-100% 13C; U-100% 15N] | 1.1 mM | |
10 | NaCl | natural abundance | 100 mM | |
11 | MES | natural abundance | 20 mM | |
12 | CaCl2 | natural abundance | 5 mM | |
13 | NaN3 | natural abundance | 0.05 % | |
14 | D2O | natural abundance | 100 % |
Solvent system 95% H2O/5% D2O, Pressure 1 atm, Temperature 293 K, pH 6.5, Details 1.1 mM [5% biosynthetically directed 13C; U-100% 15N] SlR115, 100% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
15 | SlR115 | [5% 13C; U-100% 15N] | 1.1 mM | |
16 | NaCl | natural abundance | 100 mM | |
17 | MES | natural abundance | 20 mM | |
18 | CaCl2 | natural abundance | 5 mM | |
19 | NaN3 | natural abundance | 0.05 % | |
20 | H2O | natural abundance | 95 % | |
21 | D2O | natural abundance | 5 % |