the 1H, 13C and 15N resonance assignment of ubiquitin-like small archaeal modifier protein from Haloferax volcanii
Polymer type: polypeptide(D)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 67.1 % (540 of 805) | 70.9 % (290 of 409) | 58.2 % (188 of 323) | 84.9 % (62 of 73) |
Backbone | 70.5 % (309 of 438) | 80.0 % (120 of 150) | 58.5 % (127 of 217) | 87.3 % (62 of 71) |
Sidechain | 66.1 % (288 of 436) | 65.6 % (170 of 259) | 67.4 % (118 of 175) | 0.0 % (0 of 2) |
Aromatic | 0.0 % (0 of 36) | 0.0 % (0 of 18) | 0.0 % (0 of 18) | |
Methyl | 79.2 % (84 of 106) | 83.0 % (44 of 53) | 75.5 % (40 of 53) |
1. ubiquitin-like small archaeal modifier protein
MNVTVEVVGE ETSEVAVDDD GTYADLVRAV DLSPHEVTVL VDGRPVPEDQ SVEVDRVKVL RLIKGGLEHH HHHHSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 293 K, pH 6.7
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | submit 2 | [U-100% 13C; U-100% 15N] | 1 mM | |
2 | sodium phosphate | natural abundance | 25 mM | |
3 | sodium chloride | natural abundance | 100 mM | |
4 | H2O | natural abundance | 90 % | |
5 | D2O | natural abundance | 10 % |