Solution NMR Structure of protein CD1104.2 from Clostridium difficile, Northeast Structural Genomics Consortium Target CfR130
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 89.5 % (794 of 887) | 90.2 % (414 of 459) | 88.8 % (310 of 349) | 88.6 % (70 of 79) |
Backbone | 88.5 % (400 of 452) | 88.9 % (136 of 153) | 88.4 % (199 of 225) | 87.8 % (65 of 74) |
Sidechain | 90.6 % (460 of 508) | 90.8 % (278 of 306) | 89.8 % (177 of 197) | 100.0 % (5 of 5) |
Aromatic | 60.0 % (36 of 60) | 60.0 % (18 of 30) | 60.0 % (18 of 30) | |
Methyl | 95.7 % (90 of 94) | 93.6 % (44 of 47) | 97.9 % (46 of 47) |
1. CfR130
MIRLTIEETN LLSIYNEGGK RGLMENINAA LPFMDEDMRE LAKRTLAKIA PLTENEYAEL AIFAADEVLE HHHHHHSolvent system 95% H2O/5% D2O, Pressure 1 atm, Temperature 298 K, pH 6.5, Details 1.61 mM [U-100% 13C; U-100% 15N], 95% H2O/5% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | CfR130 | [U-100% 13C; U-100% 15N] | 1.61 mM | |
2 | MES | natural abundance | 20 mM | |
3 | sodium chloride | natural abundance | 100 mM | |
4 | sodium azide | natural abundance | 0.02 % | |
5 | calcium chloride | natural abundance | 5 mM | |
6 | DTT | natural abundance | 10 mM | |
7 | DSS | natural abundance | 50 uM | |
8 | D2O | natural abundance | 5 % | |
9 | H2O | natural abundance | 95 % |
Solvent system 95% H2O/5% D2O, Pressure 1 atm, Temperature 298 K, pH 6.5, Details 1.68 mM [U-5% 13C; U-100% 15N], 95% H2O/5% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
10 | CfR130 | [U-5% 13C; U-100% 15N] | 1.68 mM | |
11 | MES | natural abundance | 20 mM | |
12 | sodium chloride | natural abundance | 100 mM | |
13 | sodium azide | natural abundance | 0.02 % | |
14 | calcium chloride | natural abundance | 5 mM | |
15 | DTT | natural abundance | 10 mM | |
16 | DSS | natural abundance | 50 uM | |
17 | D2O | natural abundance | 5 % | |
18 | H2O | natural abundance | 95 % |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.5, Details 1.68 mM [U-5% 13C; U-100% 15N] 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
19 | CfR130 | [U-5% 13C; U-100% 15N] | 1.68 mM | |
20 | MES | natural abundance | 20 mM | |
21 | sodium chloride | natural abundance | 100 mM | |
22 | sodium azide | natural abundance | 0.02 % | |
23 | calcium chloride | natural abundance | 5 mM | |
24 | DTT | natural abundance | 10 mM | |
25 | DSS | natural abundance | 50 uM | |
26 | D2O | natural abundance | 10 % | |
27 | H2O | natural abundance | 90 % | |
28 | PEG | natural abundance | 4 % |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 298 K, pH 6.5, Details 1.68 mM [U-5% 13C; U-100% 15N] 90% H2O/10% D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
29 | CfR130 | [U-5% 13C; U-100% 15N] | 1.68 mM | |
30 | MES | natural abundance | 20 mM | |
31 | sodium chloride | natural abundance | 100 mM | |
32 | sodium azide | natural abundance | 0.02 % | |
33 | calcium chloride | natural abundance | 5 mM | |
34 | DTT | natural abundance | 10 mM | |
35 | DSS | natural abundance | 50 uM | |
36 | D2O | natural abundance | 10 % | |
37 | H2O | natural abundance | 90 % | |
38 | Pf1 phage | natural abundance | 13.2 mg/mL |