1H 13C 15N resonance assignment of CD4+ T cell-derived peptide Thp5
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 63.0 % (174 of 276) | 66.4 % (95 of 143) | 53.6 % (60 of 112) | 90.5 % (19 of 21) |
Backbone | 69.8 % (88 of 126) | 88.1 % (37 of 42) | 50.8 % (33 of 65) | 94.7 % (18 of 19) |
Sidechain | 59.1 % (101 of 171) | 57.4 % (58 of 101) | 61.8 % (42 of 68) | 50.0 % (1 of 2) |
Aromatic | 56.5 % (26 of 46) | 65.2 % (15 of 23) | 45.5 % (10 of 22) | 100.0 % (1 of 1) |
Methyl | 90.0 % (18 of 20) | 90.0 % (9 of 10) | 90.0 % (9 of 10) |
1. Thp5
WRPYLQTEYY DVMTVISPPE FGSolvent system 95% H2O/5% D2O, Pressure 1 atm, Temperature 298 K, pH 6.8
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | Thp5 | natural abundance | 800 uM | |
2 | sodium chloride | natural abundance | 150 mM | |
3 | sodium phosphate | natural abundance | 50 mM | |
4 | D2O | [U-100% 2H] | 5 % | |
5 | H2O | natural abundance | 95 % |