Structure of the Cytidine Repressor DNA-Binding Domain; an alternate calculation
Polymer type: polypeptide(L)
Total | 1H | 13C | 15N | |
---|---|---|---|---|
All | 72.8 % (552 of 758) | 77.1 % (310 of 402) | 62.9 % (180 of 286) | 88.6 % (62 of 70) |
Backbone | 82.6 % (322 of 390) | 95.4 % (125 of 131) | 68.9 % (135 of 196) | 98.4 % (62 of 63) |
Sidechain | 68.1 % (294 of 432) | 68.3 % (185 of 271) | 70.8 % (109 of 154) | 0.0 % (0 of 7) |
Aromatic | 25.0 % (2 of 8) | 50.0 % (2 of 4) | 0.0 % (0 of 4) | |
Methyl | 92.9 % (65 of 70) | 91.4 % (32 of 35) | 94.3 % (33 of 35) |
1. CytR DBD
KAKKQETAAT MKDVALKAKV STATVSRALM NPDKVSQATR NRVEKAAREV GYLPQPMGRN VKRNESSolvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 308 K, pH 6.0, Details 0.411 MM [U-15N] CYTR DBD, 1.14 MM ATTTATGCAACGCA DNA, 50 MM SODIUM PHOSPHATE, 30 MM SODIUM CHLORIDE, 1 MM EDTA, 90% H2O/10 D2O
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
1 | HTH-TYPE TRANSCRIPTIONAL REPRESSOR CYTR | [U-15N] | 0.411 mM | |
2 | ATTTATGCAACGCA DNA | natural abundance | 1.14 mM | |
3 | sodium phosphate | natural abundance | 50 mM | |
4 | sodium chloride | natural abundance | 30 mM | |
5 | EDTA | natural abundance | 1 mM | |
6 | H2O | natural abundance | 90 % | |
7 | D2O | natural abundance | 10 % |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 308 K, pH 6.0
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
8 | HTH-TYPE TRANSCRIPTIONAL REPRESSOR CYTR | [U-13C; U-15N] | 1 mM | |
9 | ATTTATGCAACGCA DNA | natural abundance | 1.2 mM | |
10 | sodium phosphate | natural abundance | 50 mM | |
11 | sodium chloride | natural abundance | 30 mM | |
12 | EDTA | natural abundance | 1 mM | |
13 | H2O | natural abundance | 90 % | |
14 | D2O | natural abundance | 10 % |
Solvent system 90% H2O/10% D2O, Pressure 1 atm, Temperature 308 K, pH 6.0, Details 0.4 MM [U-15N] CYT DBD, 0.6 MM ATTTATGCAACGCA DNA, 50 MM SODIUM PHOSPHATE, 30 MM SODIUM CHLORIDE, 1 MM EDTA, 4 % C12E5 PEG/HEXANOL, 90% H2O/10%
# | Name | Isotope labeling | Type | Concentration |
---|---|---|---|---|
15 | HTH-TYPE TRANSCRIPTIONAL REPRESSOR CYTR | [U-15N] | 0.4 mM | |
16 | ATTTATGCAACGCA DNA | natural abundance | 0.6 mM | |
17 | sodium phosphate | natural abundance | 50 mM | |
18 | sodium chloride | natural abundance | 30 mM | |
19 | EDTA | natural abundance | 1 mM | |
20 | C12E5 PEG/HEXANOL | natural abundance | 4 % | |
21 | H2O | natural abundance | 90 % | |
22 | D2O | natural abundance | 10 % |